Investigation of humic acid N with X-ray photoelectron spectroscopy: Effect of acid hydrolysis and comparison with 15N cross polarization/magic angle spinning nuclear magnetic resonance spectroscopy

Organic Geochemistry

Volumn 36, Issue 11, 2005, Pages 1490-1497

  Abe, Tomonori ^a   Maie, Nagamitu ^b   Watanabe, Akira ^a  

^a NAGOYA UNIVERSITY   (Japan)

^b FLORIDA INTERNATIONAL UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AROMATIC AMINES; HUMIC ACIDS (HA); PLANT NUTRIENTS; PYROLIC NITROGEN;

AMINES; CHEMICAL BONDS; HYDROLYSIS; NITROGEN; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; NUTRITION; POLARIZATION; SOILS; X RAY PHOTOELECTRON SPECTROSCOPY;

ORGANIC ACIDS;

HUMIC SUBSTANCE; SPECTROSCOPY;

EID: 27144473621     PISSN: 01466380     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.orggeochem.2005.07.005     Document Type: Article

References (31)

1. T. Abe, and A. Watanabe X-ray photoelectron spectroscopy of nitrogen functional groups in soil humic acids Soil Science 169 2004 35 43
2. 15N CPMAS NMR-spectra of soil organic matter and composts FEBS Letters 282 1991 119 121
3. T. Asami, and M. Hara On the fractionation of soil organic nitrogen after hydrolysis using hydrochloric acid Japanese Journal of Soil Science and Plant Nutrition 41 1970 487 490 (in Japanese)
4. L. Benzing-Purdie, J.A. Ripmeester, and C.M. Preston Elucidation of the nitrogen forms in melanoidins and humic acid by nitrogen-15 cross polarization-magic angle spinning nuclear magnetic resonance Journal of Agricultural and Food Chemistry 31 1983 913 915
5. H. Bubert, J. Lambert, and P. Burba Structural and elemental investigations of isolated aquatic humic substances using X-ray photoelectron spectroscopy Fresenius' Journal Analytical Chemistry 368 2000 274 280
6. 15N NMR: origin of n-alkylnitriles in pyrolysates of ultralaminae-containing kerogens Geochimica et Cosmochimica Acta 57 1993 851 857
7. 15N-CPMAS nuclear magnetic resonance spectroscopy and biological stability of soil organic nitrogen in whole soil and particle-size fractions Organic Geochemistry 34 2003 1635 1650
8. S.J. González-Prieto, and T. Carballas Modified method for the fractionation of soil organic nitrogen by successive hydrolyses Soil Biology and Biochemistry 20 1988 1 6
9. 15N-urea and cropped to maize or pasture Plant and Soil 195 1997 151 160
10. K. Ikeya, and A. Watanabe Direct expression of an index for the degree of humification of humic acids using organic carbon concentration Soil Science and Plant Nutrition 49 2003 47 53
11. 15N NMR study of nitrogen forms in carbonaceous solids Energy and Fuels 16 2002 1507 1515
12. K.R. Kelley, and F.J. Stevenson Form and nature of organic N in soil Fertilizer Research 42 1995 1 11
13. 13C NMR spectroscopy on degraded algal residues Organic Geochemistry 31 2000 337 340
14. 15N NMR spectroscopy Australian Journal of Soil Research 38 2000 113 127
15. H. Knicker, R. Fründ, and H.-D. Lüdemann The chemical nature of nitrogen in native soil organic matter Naturwissenschaften 80 1993 219 221
16. 15N NMR spectroscopic investigation on the formation of fossil algal residues Organic Geochemistry 24 1996 661 669
17. H. Knicker, M.W.I. Schmidt, and I. Kögel-Knabner Nature of organic nitrogen in fine particle size separates of sandy soils of highly industrialized areas as revealed by NMR spectroscopy Soil Biology and Biochemistry 32 2000 241 252
18. 15N NMR spectroscopy as a tool in soil organic matter studies Geoderma 80 1997 243 270
19. K. Kumada Chemistry of Soil Organic Matter 1987 Elsevier Amsterdam
20. S. Kuwatsuka, A. Watanabe, K. Itoh, and S. Arai Comparison of two methods of preparation of humic and fulvic acids, IHSS method and NAGOYA method Soil Science and Plant Nutrition 38 1992 23 30
21. 15N-NMR study of lowland rice soils European Journal of Soil Science 51 2000 379 389
22. N. Mahieu, D.C. Olk, and E.W. Randall Multinuclear magnetic resonance analysis of two humic acid fractions from lowland rice soils Journal of Environmental Quality 31 2002 421 430
23. G.W. McCarty, J.J. Meisinger, and F.M.M. Jenniskens Relationships between total-N, biomass-N and active-N in soil under different tillage and N fertilizer treatments Soil Biology and Biochemistry 27 1995 1245 1250
24. F.J. Sowden, S.M. Griffith, and M. Schnitzer The distribution of nitrogen in some highly organic tropical volcanic soils Soil Biology Biochemistry 8 1976 55 60
25. F.J. Stevenson Organic matter in soils: pools, distribution, transformations, and function Humus Chemistry, Genesis, Composition, Reaction 1994 Wiley New York 1 23
26. K.A. Thorn, and M.A. Mikita Nitrate fixation by humic substances: nitrogen-15 nuclear magnetic resonance evidence for potential intermediates in chemodenitrification Soil Science Society of America Journal 64 2000 568 582
27. K. Tsutsuki, and S. Kuwatsuka Chemical studies on soil humic acids. III. Nitrogen distribution in humic acids Soil Science and Plant Nutrition 24 1978 561 570
28. W.J. Wang, C.J. Smith, and D. Chen Insight into the active organic nitrogen pool estimated by isotopic equilibrium approaches Soil Science Society of America Journal 67 2003 1773 1780
29. A. Watanabe, K. Itoh, S. Arai, and S. Kuwatsuka Comparison of the composition of humic and fulvic acids prepared by the IHSS method and NAGOYA method Soil Science and Plant Nutrition 40 1994 601 608
30. A. Watanabe, N. Maie, A. Hepburn, D.B. McPhail, T. Abe, K. Ikeya, Y. Ishida, and H. Ohtani Chemical characterization of Japanese Humic Substances Society standard soil humic and fulvic acids by spectroscopic and degradative analyses Humic Substances Research 1 2004 18 28
31. K. Yonebayashi, and T. Hattori Improvement in the method for fractional determination of soil organic nitrogen Soil Science and Plant Nutrition 26 1980 469 481