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a) For reviews see: a) Solladié-Cavallo, A. in Advances in Metal-Organic Chemistry, Vol 1 (Ed. Liebeskind, L. S.), JAI-Press, Greenwich, 1989, p. 99.
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b) Davies, S. G.; McCarthy, T. D. in Comprehensive Organometallic Chemistry II, Vol. 12 (Eds.: Abel, E. W.; Stone, F. G. A.; Wilkinson, G.), Pergamon Press, Oxford, 1995, p. 1039.
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27
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0026101096
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For the resolution we used a literature method: b) Bromley, L. A.; Davies, S. G.; Goodfellow, C. L. Tetrahedron Asymmetry 1991, 2, 139.
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a) Kündig, E. P.; Xu, L.-H., Romanens, P.; Bernardinelli, G. Tetrahedron Lett. 1993, 34, 7049.
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26844554322
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note
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3 group. In THF the reaction was slower (reflux, 9h, 68%).
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31
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26844537926
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note
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Longer reaction times and/or higher temperatures led to decomplexed, partially isomerized products.
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32
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26844553544
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note
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-1.
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33
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26844569678
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note
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-3. Crystallographic data for the compound Sc have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100862.
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