-
1
-
-
84973253942
-
-
(a) Francke, W.; Schröder, F.; Walter, F.; Sinnwell, V.; Baumann, H.; Kaib, M. Liebigs Ann. 1995, 965-977.
-
(1995)
Liebigs Ann.
, pp. 965-977
-
-
Francke, W.1
Schröder, F.2
Walter, F.3
Sinnwell, V.4
Baumann, H.5
Kaib, M.6
-
2
-
-
0030596997
-
-
(b) Schröder, F.; Franke, S.; Francke, W.; Baumann, H.; Kaib, M.; Pasteels, J. M.; Daloze, D. Tetrahedron 1996, 52, 13539-13546.
-
(1996)
Tetrahedron
, vol.52
, pp. 13539-13546
-
-
Schröder, F.1
Franke, S.2
Francke, W.3
Baumann, H.4
Kaib, M.5
Pasteels, J.M.6
Daloze, D.7
-
3
-
-
0029775596
-
-
(a) Schröder, F.; Sinnwell, V.; Baumann, H.; Kaib, M. J. Chem. Soc., Chem. Commun. 1996, 2139-2140.
-
(1996)
J. Chem. Soc., Chem. Commun.
, pp. 2139-2140
-
-
Schröder, F.1
Sinnwell, V.2
Baumann, H.3
Kaib, M.4
-
4
-
-
0039772279
-
-
(b) Schröder, F.; Sinnwell, V.; Baumann, H.; Kaib, M.; Francke, W. Angew. Chem., Int. Ed. Engl. 1997, 36, 77-80.
-
(1997)
Angew. Chem., Int. Ed. Engl.
, vol.36
, pp. 77-80
-
-
Schröder, F.1
Sinnwell, V.2
Baumann, H.3
Kaib, M.4
Francke, W.5
-
5
-
-
0033532006
-
-
Thanh, G. V.; Celerier, J.-P.; Lhommet, G. Tetrahedron Lett. 1999, 40, 3713-3716.
-
(1999)
Tetrahedron Lett.
, vol.40
, pp. 3713-3716
-
-
Thanh, G.V.1
Celerier, J.-P.2
Lhommet, G.3
-
7
-
-
0034608032
-
-
(a) Sayah, B.; Pelloux-Léon, N.; Vallée, Y. J. Org. Chem. 2000, 65, 2824-2826.
-
(2000)
J. Org. Chem.
, vol.65
, pp. 2824-2826
-
-
Sayah, B.1
Pelloux-Léon, N.2
Vallée, Y.3
-
8
-
-
0035815166
-
-
(b) Sayah, B.; Pelloux-Léon, N.; Milet, A.; Pardillos-Guindet, J.; Vallée, Y. J. Org. Chem. 2001, 66, 2522-2525.
-
(2001)
J. Org. Chem.
, vol.66
, pp. 2522-2525
-
-
Sayah, B.1
Pelloux-Léon, N.2
Milet, A.3
Pardillos-Guindet, J.4
Vallée, Y.5
-
9
-
-
0038738282
-
-
(c) For a formal synthesis of 3 starting with D-glutamic acid, see: Settambolo, R.; Guazzelli, G.; Lazzaroni, R. Tetrahedron: Asymmetry 2003, 14, 1447-1449.
-
(2003)
Tetrahedron: Asymmetry
, vol.14
, pp. 1447-1449
-
-
Settambolo, R.1
Guazzelli, G.2
Lazzaroni, R.3
-
10
-
-
0142183577
-
-
For recent reports on CuH-catalyzed asymmetric conjugate reduction, see: (a) Lipshutz, B. H.; Servesko, J. M. Angew. Chem., Int. Ed. 2003, 42, 4789-4792,
-
(2003)
Angew. Chem., Int. Ed.
, vol.42
, pp. 4789-4792
-
-
Lipshutz, B.H.1
Servesko, J.M.2
-
11
-
-
0042693206
-
-
and references cited therein
-
(b) Hughes, G.; Kimura, M.; Buchwald, S. L. J. Am. Chem. Soc. 2003, 126, 11253-11258 and references cited therein.
-
(2003)
J. Am. Chem. Soc.
, vol.126
, pp. 11253-11258
-
-
Hughes, G.1
Kimura, M.2
Buchwald, S.L.3
-
13
-
-
0033537956
-
-
(d) Mori, A.; Fujita, A.; Kajiro, H.; Nishihara, Y.; Hiyama, T. Tetrahedron 1999, 55, 4573-4582.
-
(1999)
Tetrahedron
, vol.55
, pp. 4573-4582
-
-
Mori, A.1
Fujita, A.2
Kajiro, H.3
Nishihara, Y.4
Hiyama, T.5
-
14
-
-
1942533561
-
-
Rainka, M. P.; Aye, Y.; Buchwald, S. L. Proc. Nat. Acad. Sci. U.S.A. 2004, 101, 5821-5823.
-
(2004)
Proc. Nat. Acad. Sci. U.S.A.
, vol.101
, pp. 5821-5823
-
-
Rainka, M.P.1
Aye, Y.2
Buchwald, S.L.3
-
15
-
-
84993918914
-
-
Ester 13 is commercially available and can be prepared on > 30-g scale; see: Drinan, M. A.; Lash, T. D. J. Heterocycl. Chem. 1994, 31, 255-257.
-
(1994)
J. Heterocycl. Chem.
, vol.31
, pp. 255-257
-
-
Drinan, M.A.1
Lash, T.D.2
-
16
-
-
85083270067
-
-
Ohta, S.; Shimabayashi, A.; Hayakawa, S.; Sumino, M.; Okamoto, M. Synthesis 1985, 45-48.
-
(1985)
Synthesis
, pp. 45-48
-
-
Ohta, S.1
Shimabayashi, A.2
Hayakawa, S.3
Sumino, M.4
Okamoto, M.5
-
18
-
-
0001038733
-
-
For reviews, see: (a) Wolfe, J. P.; Wagaw, S.; Marcoux, J.-F.; Buchwald, S. L. Acc. Chem. Res. 1998, 31, 805-818.
-
(1998)
Acc. Chem. Res.
, vol.31
, pp. 805-818
-
-
Wolfe, J.P.1
Wagaw, S.2
Marcoux, J.-F.3
Buchwald, S.L.4
-
22
-
-
0000664403
-
-
For the synthesis of Z-β-iodoenoates, see: (a) Piers, E.; Wong, T.; Coish, P. D.; Rogers, C. Can. J. Chem. 1994, 72, 1816-1819.
-
(1994)
Can. J. Chem.
, vol.72
, pp. 1816-1819
-
-
Piers, E.1
Wong, T.2
Coish, P.D.3
Rogers, C.4
-
23
-
-
0031021265
-
-
(b) Rossi, R.; Bellina, F.; Mannina, L. Tetrahedron 1997, 53, 1025-1044.
-
(1997)
Tetrahedron
, vol.53
, pp. 1025-1044
-
-
Rossi, R.1
Bellina, F.2
Mannina, L.3
-
24
-
-
0027180141
-
-
For reviews on the preparation and use of vinyl triflates, see: (a) Ritter, K. Synthesis 1993, 735-762.
-
(1993)
Synthesis
, pp. 735-762
-
-
Ritter, K.1
-
25
-
-
0034640532
-
-
(b) Baraznenok, I. L.; Nenajdenko, V. G.; Balenkova, E. S. Tetrahedron 2000, 56, 3077-3119.
-
(2000)
Tetrahedron
, vol.56
, pp. 3077-3119
-
-
Baraznenok, I.L.1
Nenajdenko, V.G.2
Balenkova, E.S.3
-
26
-
-
0034714545
-
-
(a) Tomori, H.; Fox, J. M.; Buchwald, S. L. J. Org. Chem. 2000, 65, 5334-5341.
-
(2000)
J. Org. Chem.
, vol.65
, pp. 5334-5341
-
-
Tomori, H.1
Fox, J.M.2
Buchwald, S.L.3
-
27
-
-
26444570992
-
-
XPhos is available from Strem Chemicals, Inc.
-
(b) XPhos is available from Strem Chemicals, Inc.
-
-
-
-
28
-
-
0002261207
-
-
For palladium-catalyzed N-vinylation of lithiated azoles, see: (a) Lebedev, A. Y.; Izmer, V. V.; Kazyul'kin, D. N.; Beletskaya, I. P.; Voskoboynikov, A. Z. Org. Lett. 2002, 4, 623-626.
-
(2002)
Org. Lett.
, vol.4
, pp. 623-626
-
-
Lebedev, A.Y.1
Izmer, V.V.2
Kazyul'kin, D.N.3
Beletskaya, I.P.4
Voskoboynikov, A.Z.5
-
29
-
-
0347411032
-
-
For recent reports on palladium-catalyzed N-vinylation, see: (b) Wallace, D. J.; Klauber, D. J.; Chen, C.-y.; Volante, R. P. Org. Lett. 2003, 5, 4749-4752, and
-
(2003)
Org. Lett.
, vol.5
, pp. 4749-4752
-
-
Wallace, D.J.1
Klauber, D.J.2
Chen, C.-Y.3
Volante, R.P.4
-
30
-
-
18244388691
-
-
(c) Klapars, A.; Campos, K. R.; Chen, C.-y.; Volante, R. P. Org. Lett. 2005, 7, 1185-1188.
-
(2005)
Org. Lett.
, vol.7
, pp. 1185-1188
-
-
Klapars, A.1
Campos, K.R.2
Chen, C.-Y.3
Volante, R.P.4
-
34
-
-
0037708569
-
-
(d) Drexler, H.-J.; You, J.; Zhang, S.; Fischer, C.; Baumann, W.; Spannenberg, A.; Heller, D. Org. Proc. Res. Dev. 2003, 7, 355-361.
-
(2003)
Org. Proc. Res. Dev.
, vol.7
, pp. 355-361
-
-
Drexler, H.-J.1
You, J.2
Zhang, S.3
Fischer, C.4
Baumann, W.5
Spannenberg, A.6
Heller, D.7
-
36
-
-
26444477071
-
-
note
-
The ee was determined by chiral HPLC analysis of a more advanced intermediate.
-
-
-
-
37
-
-
26444518869
-
-
note
-
Please see Supporting Information for details.
-
-
-
-
38
-
-
26444451764
-
-
note
-
5
-
-
-
-
39
-
-
0004267670
-
-
Wiley: New York
-
For reviews on the chemistry of pyrroles, see: (a) Pyrroles; Jones, A., Ed.; Wiley: New York, 1990,
-
(1990)
Pyrroles
-
-
Jones, A.1
-
42
-
-
26444467805
-
-
note
-
Compounds not containing the C8-carbonyl in this series were found to be less stable toward storage as a result of decomposition and polymerization.
-
-
-
-
43
-
-
0030840135
-
-
(a) Aldabbagh, F.; Bowman, W. R.; Mann, E. Tetrahedron Lett. 1997, 38, 7937-7940.
-
(1997)
Tetrahedron Lett.
, vol.38
, pp. 7937-7940
-
-
Aldabbagh, F.1
Bowman, W.R.2
Mann, E.3
-
44
-
-
0033215458
-
-
(b) Miranda, L. D.; Cruz-Almanza, R.; Pavón, M.; Alva, E.; Muchowski, J. M. Tetrahedron Lett. 1999, 40, 7153-7157.
-
(1999)
Tetrahedron Lett.
, vol.40
, pp. 7153-7157
-
-
Miranda, L.D.1
Cruz-Almanza, R.2
Pavón, M.3
Alva, E.4
Muchowski, J.M.5
-
45
-
-
0035968964
-
-
(c) Allin, S. M.; Barton, W. R. S.; Bowman, R.; McInally, T. Tetrahedron Lett. 2001, 42, 7887-7890.
-
(2001)
Tetrahedron Lett.
, vol.42
, pp. 7887-7890
-
-
Allin, S.M.1
Barton, W.R.S.2
Bowman, R.3
McInally, T.4
-
46
-
-
0001044813
-
-
(a) Nakamura, E.; Inubushi, T.; Aoki, S.; Machii, D. J. Am. Chem. Soc. 1991, 113, 8980-8982.
-
(1991)
J. Am. Chem. Soc.
, vol.113
, pp. 8980-8982
-
-
Nakamura, E.1
Inubushi, T.2
Aoki, S.3
Machii, D.4
-
47
-
-
2442699005
-
-
(b) Menes-Arzate, M.; Martínez, R.; Cruz-Almanza, R.; Muchowski, J. M.; Osonio, Y. M.; Miranda, L. D. J. Org. Chem. 2004, 69, 4001-4004.
-
(2004)
J. Org. Chem.
, vol.69
, pp. 4001-4004
-
-
Menes-Arzate, M.1
Martínez, R.2
Cruz-Almanza, R.3
Muchowski, J.M.4
Osonio, Y.M.5
Miranda, L.D.6
-
49
-
-
26444501131
-
-
note
-
The immediate air oxidation product of myrmicarins 215A, 215B, and 217 corresponds to myrmicarins 213A, 213B, and 215C, respectively.
-
-
-
-
51
-
-
26444455727
-
-
note
-
More forcing dehydration conditions and longer reaction times resulted in lower mass recovery and complications involving C6-C7 oxidation.
-
-
-
-
52
-
-
26444516177
-
-
note
-
Direct acidification of the reaction mixture can also provide myrmicarin 215B. See Supporting Information for details.
-
-
-
|