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n ∼ 90 000 g/mol) was prepared by the anionic polymerization of α,α′-dibromo2,5- di(2′-ethylhexyloxy)xylene as described by: Neef, C. J.; Ferraris, J. P. Macromolecules 2000, 33, 2311-2314. The synthesis of the monomer was accomplished in two steps from hydroquinone. The hydroquinone reaction with 2′-ethylhexyl bromide (for details of this etherification see ref 51) was followed by a treatment with paraformaldehyde as described by Neef et al. To control the molecular weight, we used 1 mol % of the initiator (method B). The two additional precipitations were from toluene (0.5 wt %) into acetone/methanol (1:1).
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