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note
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2 groups of the THF molecules. The positions of the hydrogen atoms could be calculated using riding models for all carbon atoms, except the disordered ones. The high R factor is due to poorly diffracting single crystals and the disorder effect. Crystallographic data for the structure reported here have been deposited with the Cambridge Crystallographic Data Centre as Supplementary Publication No. CCDC-255330. Copies of the data can be obtained free of charge on application to the CCDC, 12 Union Road, Cambridge CB21EZ, U.K. (fax, (+44)1223-336-033; e-mail, deposit@ ccdc.cam.ac.uk).
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