Fast temperature cycling in microstructure devices

Chemical Engineering Journal

Volumn 101, Issue 1-3, 2004, Pages 217-224

  Brandner, J J ^a   Emig, G ^b   Liauw, M A ^c   Schubert, K ^a  

^a KARLSRUHE INSTITUTE OF TECHNOLOGY   (Germany)

^b UNIVERSITY OF ERLANGEN NUREMBERG   (Germany)

^c RWTH AACHEN UNIVERSITY   (Germany)

Author keywords

Microstructure reactor; Periodic process; Temperature modulation; Unsteady state

Indexed keywords

CATALYSTS; CHEMICAL REACTORS; COOLING; HEATING; MICROSTRUCTURE; REACTION KINETICS; THERMODYNAMIC STABILITY;

MICROSTRUCTURE DEVICES;

THERMAL CYCLING;

PROCESS CONTROL APPLICATION; TEMPERATURE CONTROL;

EID: 2542500786     PISSN: 13858947     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cej.2003.11.020     Document Type: Article

References (23)

1. Bailey J.E.Periodic operation of chemical reactors: a review Chem. Eng. Commun. 1 1973 111-124
2. P.L. Silveston, Composition Modulation of Catalytic Reactors, Gordon and Breach, Amsterdam, 1998.
3. J.J. Brandner, G. Emig, M. Fichtner, M.A. Liauw, K. Schubert, A new microstructure device for fast temperature cycling for chemical reactions, in: M. Matlosz, W. Ehrfeld, J.P. Baselt (Eds.), Proceedings of the Fifth International Conference on Microreaction Technology, IMRET 5, Springer, Berlin, 2001, pp. 164-174.
4. Rouge A.Spoetzl B.Gebauer K.Schenk R.Renken A.Microchannel reactors for fast periodic operation: the catalytic dehydration of isopropanol Chem. Eng. Sci. 56 2001 1419-1427
5. 2 gas thermocycler Gen. Eng. News 2211 2002 42-43
6. Silveston P.L.Hudgins R.R.Renken A.Periodic operation of catalytic reactors-introduction and overview Catal. Today 25 1995 91-112
7. Van Neer F.J.R.Kodde A.J.Den Uil H.Bliek A.Understanding of resonance phenomena on a catalyst under forced concentration and temperature oscillations Can. J. Chem. Eng. 74 1996 664-673
8. Schubert K.Brandner J.J.Fichtner M.Linder G.Schygulla U.Wenka A.Microstructure devices for applications in thermal and chemical process engineering Microscale Thermophys. Eng. 51 2001 17-39
9. J.J. Brandner, M. Fichtner, K. Schubert, Electrically heated microstructure heat exchangers and reactors, in: W. Ehrfeld (Ed.), Proceedings of the Third International Conference on Microreaction Technology: Industrial Prospects, IMRET 3, 1999, Springer, Berlin, 2000, pp. 607-616.
10. V. Hessel, H. Löwe, Mikroverfahrenstechnik: Komponenten-Anlagenkonzeption-Anwenderakzeptanz, CIT 74 (2002)
11. Hessel V.Löwe H.Mikroverfahrenstechnik: Komponenten-Anlagenkonzeption-Anwenderakzeptanz CIT 1-2 2002 17-30
12. Hessel V.Löwe H.Mikroverfahrenstechnik: Komponenten-Anlagenkonzeption-Anwenderakzeptanz CIT 3 2002 185-207
13. Hessel V.Löwe H.Mikroverfahrenstechnik: Komponenten-Anlagenkonzeption-Anwenderakzeptanz CIT 4 2002 381-400
14. K. Schubert, W. Bier, J.J. Brandner, M. Fichtner, C. Franz, G. Linder, Realization and testing of microstructure reactors, microheat exchangers and micromixers for industrial applications in chemical engineering, in: Process Miniaturization, Proceedings of the Second International Conference on Microreaction Technology, AIChE Topical Conference Preprints, 1998, pp. 88-95.
15. Haas-Santo K.Fichtner M.Schubert K.Preparation of microstructure compatible porous supports by sol-gel synthesis for catalyst coatings Appl. Catal. A 220 2001 79-92
16. J.J. Brandner, Entwicklung von Mikrostrukturreaktoren zum thermisch instationären Betrieb chemischer Reaktionen, Ph.D. Thesis, Universität Karlsruhe (TH), Wissenschaftliche Berichte des Forschungszentrum Karlsruhe FZKA 6891, 2003.
17. Ch. Alépée, R. Maurer, L. Paratte, L. Vulpescu, Ph. Renaud, A. Renken, Fast heating and cooling for high temperature chemical microreactors, in: W. Ehrfeld (Ed.), Proceedings of the Third International Conference on Microreaction Technology: Industrial Prospects, IMRET 3, 1999, Springer, Berlin, 2000, pp. 514-525.
18. S. Poser, R. Ehricht, T. Schulz, S. Uebel, U. Dillner, J.M. Köhler, Rapid PCR in flow-through Si chip thermocyclers, in: W. Ehrfeld (Ed.), Proceedings of the Third International Conference on Microreaction Technology: Industrial Prospects, IMRET 3, 1999, Springer, Berlin, 2000, pp. 410-419.
19. J.J. Brandner, G. Emig, M.A. Liauw, K. Schubert, Fast temperature cycling with microstructure devices, in: J.P. Baselt (Ed.), Proceedings of the Sixth International Conference on Microreaction Technology, AIChE, 2002, pp. 275-280.
20. K.P. Brooks, S.D. Rassat, R.S. Wegeng, V.S. Stenkamp, W.E. TeGrotenhuis, D.D. Caldwell, Component development for a microchannel in situ propellant system, in: J.P. Baselt (Ed.), Proceedings of the Sixth International Conference on Microreaction Technology, AIChE, 2002, pp. 219-229.
21. 3-Beschichtungen in Mikrokanälen von komplett gefertigten Mikrostrukturreaktoren Chem. Ing. Techn. 73 2001 1168-1172
22. K. Haas-Santo, O. Görke, K. Schubert, J. Fiedler, H. Funke, A microstructure reactor system for the controlled oxidation of hydrogen for possible application in space, in: M. Matlosz, W. Ehrfeld, J.P. Baselt (Eds.), Proceedings of the Fifth International Conference on Microreaction Technology, IMRET 5, Springer, Berlin, 2001, pp. 313-321.
23. O. Görke, P. Pfeifer, K. Schubert, Determination of kinetic data of exothermic reactions in the isothermal microstructure reactor based on the example of catalyzed oxidation of hydrogen, in: J.P. Baselt (Ed.), Proceedings of the Sixth International Conference on Microreaction Technology, AIChE, 2002, pp. 262-272.