Crystal structure of molybdenum and tungsten trans-bis(dinitrogen)-bis{bis(di(p-ethylbenzene)phosphino)ethane} toluene solvate, M(C34H40P2)2(N 2)2 · C7H8 (M = Mo, W)

Zeitschrift fur Kristallographie - New Crystal Structures

Volumn 219, Issue 3, 2004, Pages 249-254

  Zeller, M ^a   Hunter, A D ^a  

^a YOUNGSTOWN STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 24644437402     PISSN: 14337266     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (16)

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2. Herbstein, F. H.: How precise are measurements of unit-cell dimensions from single crystals? Acta Crystallogr. B56 (2000) 547-557.
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4. 3]. J. Am. Chem. Soc. 105 (1983) 3014-3022.
5. 6). Acta Crystallogr. C41 (1985) 1017-1019.
6. Pietsch, B.; Dahlenburg, L.: Oligophosphine ligands. XVII. trans-Bis(dinitrogen)-mer-[bis(3-diphenylphosphinopropyl)phenylphosphine] (trimethylphosphine)molybdenum(0). Acta Crystallogr. C42 (1986) 995-997.
7. 3]. J. Chem. Soc., Chem. Commun. (1984) 958-958.
8. Anderson, S. N.; Hughes, D. L.; Richards, R. L.: Preparation of mer-tris(dinitrogen-N)tris(dipropylphenylphosphine)molybdenum from transbis(dinitrogen-N)tetrakis(dipropylphenylphosphine) molybdenum; its x-ray crystal structure, spectroscopic properties, and protonation to give ammonia. J. Chem. Soc., Dalton Trans. (1986) 1591-1994.
9. Anderson, S. N.; Richards, R. L.; Hughes, D. L.: Preparation and crystal structure of (μ-dimtrogen)bis[bis(dinkrogen)(diethylphenylphosphine)tungsten] (μ-dinitrogen). J. Chem. Soc., Chem. Commun. (1982) 1291-1292.
10. 2] (M = molybdenum or tungsten), and the crystal structure of cis-tetrakis(dimethylphenylphosphine)bis(dinitrogen)tungsten. J. Chem. Soc., Dalton Trans. (1985) 1523-1526.
11. Wagner, T; Englert, U.: Packing effects in organometallic compounds: a study of five mixed crystals. Struct. Chem. 8 (1997) 357-365.
12. Hu, C.; Hodgeman, W. C.; Bennett, D. W.: Bis(1,2-bis(diphenylphosphino)ethane)tungsten(0) Complexes Containing Electron-Saturated Metal Centers and Singly-Coordinated Bridging Ligands. Inorg. Chem. 35 (1996) 1621-1626.
13. Uchida, T.; Uchida, Y.; Hidai, M.; Kodama, T.: trans-Bis(dinitrogen)bis[1,2-bis(diphenylphosphino)elhane]molybdenum(0). Acta Cryst. B31 (1975) 1197-1199.
14. Dilworth, J. R.; Richards, R. L.: The Synthesis of Molybdenum and Tungsten Dinitrogen Complexes. Inorg. Synth. 20 (1980) 119-127.
15. Sheldrick, G. M.: SHELXS-97. Program for the Solution of Crystal Structures. University of Göttingen, Germany 1997.
16. Sheldrick, G. M.: SHELXL-97. Program for the Refinement of Crystal Structures. University of Göttingen, Germany 1997.