Adaptation of a color reaction for spectrophotometric determination of diclofenac sodium and piroxicam in pure form and in pharmaceutical formulations

Analytical Letters

Volumn 37, Issue 6, 2004, Pages 1151-1162

  El Didamony, A M ^a   Amin, A S ^b  

^a Zagazig University   (Egypt)

^b BENHA UNIVERSITY   (Egypt)

Author keywords

Diclofenac sodium; Pharmaceutical formulations; Piroxicam; Spectrophotometry

Indexed keywords

1,10 PHENANTHROLINE; ACETIC ACID; BUFFER; DECLOPHEM; DICLOFENAC; IRON; IRON COMPLEX; PIROXICAM; TRIS(1,10 PHENANTHROLINE); UNCLASSIFIED DRUG;

AMPOULE; ARTICLE; COLOR; COMPLEX FORMATION; CONCENTRATION (PARAMETERS); DRUG CAPSULE; DRUG DETERMINATION; DRUG FORMULATION; OXIDATION; PH; POWDER; SENSITIVITY AND SPECIFICITY; SPECTROPHOTOMETRY; SUPPOSITORY; TABLET; THEORY;

EID: 2442661639     PISSN: 00032719     EISSN: None     Source Type: Journal    
DOI: 10.1081/AL-120034060     Document Type: Article

References (40)

1. Reynolds, J.E.F. The Extra Pharmacopoeia "Martindale," 30th Ed.; The Pharmaceutical Press: London, 1982; 250.
2. Florey, K. Analytical Profile of Drug Substances; Academic Press: London, 1981; Vol. 15, 509-531.
3. Supplement 2 to the United States Pharmacopeia, 24th Rev.; The National Formulary, 19th Rev;. The United States Pharmacopeial Convention: Rockville, MD, 2000.
4. Chen, X.; Xi, N.; Ge, S.; Sun, S. HPLC determination of piroxicam in human serum and its pharmacokinetic parameters. Yaoxue Xuebao 1986, 21 (9), 692-697.
5. Ge, S.; Cheng, Q.; Wang, X.; Xi, N. High-performance liquid chromatography determination of piroxicam contents in piroxicam suppositories. Yaoxue Xuebao 1988, 23 (1), 38-41.
6. Jiang, X.; Ge, S.; Wang, X.; Xi, N. High-performance liquid chromatography method for determining piroxicam in body fluids. Zhongguo Yaoli Xuebao 1991, 12 (4), 381-384.
7. Maya, M.T.; Pais, J.P.; Morais, J.A. A rapid method for the determination of piroxicam in plasma by high-performance liquid chromatography. J. Pharm. Biomed. Anal. 1995, 13 (3), 319-322.
8. Chen, H.; Mi, Z.Y.; Liu, W.Z. Study on an high-performance liquid chromatography method for the determination of piroxicam in gels. Fenxi Kexuse Xuebao 2000, 16 (6), 470-473.
9. Gaudiano, M.C.; Valvo, L.; Bertocchi, P.; Manna, L. RP-HPLC study of the degradation of diclofenac and piroxicam in the presence of hydroxyl radicals. J. Pharm. Biomed. Anal. 2003, 32 (1), 151-158.
10. Kumar, Y.; Talwar, S.K.; Rathore, Y.K.S.; Sethi, P.D.; Jain, C.L. Spectrophotometric estimation of piroxicam in pharmaceutical formulations through cobalt(II) and copper(II) chelation. Indian Drugs 1990, 28 (3), 139-141.
11. Sánchez-Pedreńo, C.; Garcia, M.S.; Albero, M.I.; Rodriguez, J. Flow injection spectrophotometric determination of piroxicam. J. Pharm. Biomed. Anal. 1993, 11 (10), 933-938.
12. Ródenas, V.; Garcia, M.S.; Sánchez-Pedreńo, C.; Albero, M.I. Simultaneous determination of piroxicam and its major metabolite 5-hydroxypiroxicam in human plasma by derivative spectrophotometry. Analyst 1998, 123 (8), 1749-1752.
13. Klopas, A.; Panderi, I.; Parissi-Poulou, M. Determination of piroxicam and its major metabolite 5-hydroxypiroxicam in human plasma by zero-crossing first-derivative spectrophotometry. J. Pharm. Biomed. Anal. 1998, 17 (3), 515-524.
14. Amin, A.S. Spectrophotometric determination of piroxicam and tenoxicam in pharmaceutical formulations using alizarin. J. Pharm. Biomed. Anal. 2002, 29 (4), 729-736.
15. Gowda, B.G.; Seetharamappa, J.; Melwanki, M.B. Indirect spectrophotometric determination of propranolol hydrochloride and piroxicam in pure and pharmaceutical formulations. Anal. Sci. 2002, 18 (6), 671-674.
16. El Ries, M.A.; Mohamed, G.; Khalil, S.; El Shall, M. Spectrophotometric and potentiometric determination of piroxicam and tenoxicam in pharmaceutical preparations. Chem. Pharm. Bull. 2003, 51 (1), 6-10.
17. Escandar, G.M. Spectrofluorimetric determination of piroxicam in the presence and absence of β-cyclodextrin. Analyst 1999, 124 (4), 587-591.
18. Acuńa, J.A.; De La Fuente, C.; Vázquez, D.M.; Tascón, M.L.; Sánchez-Batanero, P. Voltammetric determination of piroxicam in micellar media by using conventional and surfactant chemically modified carbon paste electrodes. Talanta 1993, 40 (11), 1637-1642.
19. Paniagua, A.R.; Vazquez, M.D.; Tascon, M.L.; Sanchez-Batanero, P. Voltammetric determination of piroxicam after incorporation within carbon pastes. Electroanalysis 1994, 6 (3), 265-268.
20. Gonzalez, M.; Vazquez, M.D.; Tascon, M.L.; Sanchez-Batanero, P. Contribution to the electrochemical behaviour study of piroxicam in different aqueous-organic media and electrodes by using polarographic and voltammetric techniques. Electroanalysis (N.Y.) 1994, 6 (5-6), 497-504.
21. Shinde, V.M.; Tendolkar, N.M.; Desai, B.S. Simultaneous determination of paracetamol and diclofenac sodium in pharmaceutical preparation by quantitative TLC. J. Planar Chromatogr.- Mod. TLC 1994, 7 (1), 50-53.
22. Sun, S.W.; Fabre, H. Practical approach for validating the TLC assay of an active ingredient in pharmaceutical formulation. J. Liq. Chromatogr. 1994, 17 (2), 433-445.
23. Chawla, J.L.; Sodhi, R.A.; Sane, R.T. Simultaneous determination of chlorzoxazone, paracetamol, and diclofenac sodium by different chromatographic techniques. Indian Drugs 1996, 33 (4), 171-178.
24. Miller, R.B. High-performance liquid-chromatographic determination of diclofenac in human plasma using automated column switching. J. Chromatogr., Biomed. Appl. 1993, 127 ((2) J. Chromatogr. 616), 283-290.
25. Kubala, T.; Gambhir, B.; Borst, S.I. Specific stability indicating high-performance liquid chromatography method to determine diclofenac sodium in raw materials and pharmaceutical solid dosage forms. Drug Dev. Ind. Pharm. 1993, 19 (7), 749-757.
26. Li, K.; Zhao, F.L.; Yuan, Y.S.; Tan, L. Determination of diclofenac sodium in human plasma by RP-HPLC. Yaowu Fenxi Zazhi 1995, 15 (5), 17-19.
27. Giagoudakis, G.; Markantonis, S.L. An alternative high-performance liquid-chromatographic method for the determination of diclofenac and flurbiprofen in plasma. J. Pharm. Biomed. Anal. 1998, 17 (4-5), 897-901.
28. Lala, L.; D'Mello, P.M.; Naik, S.R. HPTLC determination of diclofenac sodium from serum. J. Pharm. Biomed. Anal. 2002, 29 (3), 539-544.
29. Mathur, S.C.; Kumar, Y.; Prasad, P.B.N.; Rao, A.C.S.; Rathore, Y.K.S.; Gupta, S.C. A simple colorimetric estimation of diclofenac sodium in dosage forms. Indian Drugs 1994, 31 (9), 447-448.
30. Prado, M.S.A.; Steppe, M.; Tavares, M.F.M.; Kedor-Hackmann, E.R.M.; Santoro, M.I.R.M. Method validation for diclofenac sodium in pharmaceutical by capillary electrophoresis. J. Capillary Electrophor. 1999, 6 (3-4), 125-129.
31. Agrawal, Y.K.; Upadhyay, V.P.; Menon, S.K. Spectrophotometric determination of diclofenac sodium. Indian J. Pharm. Sci. 1988, 50 (1), 58-60.
32. Agrawal, Y.K.; Shivramchandra, K. Spectrophotometric determination of diclofenac sodium in tablets. J. Pharm. Biomed. Anal. 1991, 9 (2), 97-100.
33. Kamath, B.V.; Shivram, K.; Oza, G.P.; Vangani, S. Use of charge transfer complexation in the spectrophotometric determination of diclofenac sodium. Anal. Lett. 1993, 26 (4), 665-674.
34. Kamath, B.V.; Shivram, K. Spectrophotometric determination of diclofenac sodium via oxidation reactions. Anal. Lett. 1993, 26 (5), 903-911.
35. Botello, J.C.; Pérez-Caballero, G. Spectrophotometric determination of diclofenac sodium with methylene blue. Talanta 1995, 42 (1), 105-108.
36. Perez-Ruiz, T.; Martinez-Lozano, C.; Sanz, A.; San Miguel, M.T. Flow extraction spectrophotometric method for the determination of diclofenac sodium in pharmaceutical preparations. J. Pharm. Biomed. Anal. 1997, 16 (2), 249-254.
37. Fernández de Córdova, M.L.; Ortega-Barrales, P.; Molina Diaz, A. Sensitive and selective determination of diclofenac sodium in pharmaceutical preparations by solid phase ultraviolet absorptiometry. Anal. Chim. Acta 1998, 369 (3), 263-268.
38. Ortega-Barrales, P.; Ruiz-Medina, A.; Fernandez-De Cordova, M.L.; Molina-Diza, A. Senstive and simple determination of diclofenac sodium by use of a continuous flow-injection procedure with solid-phase spectroscopic detection. Anal. Sci. 1999, 15 (10), 985-989.
39. Britton, H.T.S. Hydrogen Ions, 4th Ed.; Chapman and Hall; 1952.
40. Miller, C.; Miller, J.N. Significance tests. In Statistics in Analytical Chemistry, 3th Ed.; Ellis Horwood: Chichester, 1993; Chapter 3.