Method development and selectivity optimization in high-Performance liquid chromatography

Advances in Chromatography

Volumn 39, Issue , 1998, Pages 263-309

  Billiet, H A H ^a   Rippel, G ^a,b  

^a DELFT UNIVERSITY OF TECHNOLOGY   (Netherlands)

^b BUDAPEST UNIVERSITY OF TECHNOLOGY AND ECONOMICS   (Hungary)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 24144495857     PISSN: 00652415     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (76)

1. P. Csokán, K. Valkó, F. Darvas, and F. Csizmadia, LC-GC, 6: 361 (1993).
2. G. Szepesi and K. Valkó, Prediction of initial high-performance liquid chromatographic conditions for selectivity optimization in pharmaceutical analysis by an expert system approach. J. Chromatogr., 550: 87-100 (1991).
3. J. Fekete, G. Morovján, F. Csizmadia, and F. Darvas, Method development by an expert system: Advantages and limitations, J. Chromatogr. A, 660: 33-46 (1994).
4. S. V. Galushko, Calculation of retention and selectivity in reversed-phase liquid chromatography, J. Chromatogr., 552, 91-102 (1991).
5. S. V. Galushko, Calculation of retention and selectivity in reversed-phase liquid chromatography. II. Methanol-water eluents, Chromatographia, 36: 39-42 (1993).
6. S. V. Galushko, A. A. Kamenchuk, and G. L. Pit, Calculation of retention in reversed-phase liquid chromatography. IV. ChromDream software for the selection of initial conditions and for simulating chromatographic behavior, J. Chromatogr. A, 660: 47-59 (1994).
7. J. A. Lewis, D. C. Lommen, W. D. Raddatz, J. W. Dolan, L. R. Snyder, and I. Molnar, Computer simulation for the prediction of separation as a function of pH for reversed-phase high-performance liquid chromatography. I. Accuracy of a theory-based model, J. Chromatogr., 592: 183-195 (1992).
8. J. A. Lewis, J. W. Dolan, and L. R. Snyder, Computer simulation for the prediction of separation as a function of pH for reversed-phase high-performance liquid chromatography. II. Resolution as a function of simultaneous change in pH and solvent strength. J. Chromatogr., 592: 197-208 (1992).
9. P. J. Schoenmakers, N. Mackie, and R. M. Lopes Marques, Optimizing separations in reversed phase liquid chromatogra-phy by varying pH and solvent composition, Chromatographia, 35: 18-32 (1993).
10. Peter J. Schoenmakers, Sylvie van Molle, Carmel M. G. Hayes, and Louis G. M. Uunk, Effects of pH in reversed-phase liquid chromatography, Anal. Chim. Acta, 250: 1-19 (1991).
11. Rui M. lopes Marques and Peter J. Schoenmakers, Modeling retention in reversed-phase liquid chromatography as a function of pH and solvent composition, J. Chromatogr., 592: 157-182 (1992).
12. Margriet Hendriks, Non-linear retention modeling in liquid chromatography, Ph.D. thesis, University of Groningen, April 1996.
13. B. Bourguignon, F. Marcenac, H. R. Keller, P. F. de Aguiar, and D. L. Massart, Simultaneous optimization of pH and organic modifier content of the mobile phase for the separation of chlorophenols using a Doehlert design, J. Chromatogr., 628: 171-189 (1993).
14. P. J. Schoenmakers, Optimization of Chromatographic Selectivity: A Guide to Method Development, Journal of Chromatography library, vol. 35, Elsevier, Amsterdam, 1986, p. 51.
15. K. Valko, L. R. Snyder, and J. L. Glajch, Retention in reversed-phase liquid chromatography as a function of mobile-phase composition, J. Chromatogr. A, 656: 501-520 (1993).
16. A. K. Smilde, P. M. J. Coenegracht, C. H. P. Bruins, and D. A. Doornbos, Multivariate calibration strategy for reversed-phase chromatographic systems based on the characterization of stationary-mobile phase combinations with markers, J. Chromatogr., 485: 169-181 (1989).
17. L. de Galan, H. A. H. Billiet, Mobile Phase Optimization in RPLC by an Iterative Regression Design, Advances in Chromatography, vol. 25, Marcel Dekker, New York, 1986, pp. 63-104.
18. H. A. H. Billiet and L. de Galan, Selection of mobile phase parameters and their optimization in reversed-phase liquid chromatography, J. Chromatogr., 485: 27-50 (1989).
19. L.. R. Snyder and J. W. Dolan, Initial experiments in high-performance liquid chromatographic method development I. Use of starting gradient run. J. Chromatogr. A, 721: 3-14 (1996).
20. J. A. Lewis, L. R. Snyder, and J. W. Dolan, Initial experiments in high-performance liquid chromatographic method development II. Recommended approach and conditions for isocratic separation. J. Chromatogr. A, 721: 15-29 (1996).
21. T. Hamoir and D. L. Massart, Strategic approach for the method selection in high-performance liquid chromatography. Anal. Chim. Acta, 298: 319-329 (1994).
22. T. Hamoir, B. Bourguignon, and D. L. Massart, Validation of a strategic approach to high-performance liquid chromatographic method selection, Chromatographia, 39: 339-345 (1994).
23. G. K. Low, A. Bartha, H. A. H. Billiet, and L. de Galan, A systematic procedure for the determination of the nature of the solutes prior to the selection of the mobile phase parameters for optimization of reversed-phase ion-pair chromatographic separations, J. Chromatogr., 478: 21 (1989).
24. A. Bartha and Gy. Vigh, Rule-based approach for the determination of solute types in unknown sample mixtures as a first step of optimization parameter selection in reversed-phase ion-pair chromatography, J. Chromatogr., 485: 383-401 (1989).
25. A. Peters, L. Buydens, D. L. Massart, and P. J. Schoenmakers, An expert system for the selection of criteria for the selectivity optimization in high pressure liquid chromatography, Chromatographia, 26, 101-109 (1988).
26. N. Hadden, F. Baumann, F. MacDonald, M. Munk, R. Stevenson, D. Gere, F. Zamaroni, and R. Majors, Basic Liquid Chromatography, Varian Aerograph, 1971, p. 4-27.
27. A. Bartha, H. A. H. Billiet, L. de Galan, The evaluation and sequential use of resolution based criteria in the optimization of the separation of a limited subset of components by HPLC, J. Liq. Chromatog., 12: 173-197 (1989).
28. M. M. W. B. Hendriks, J. H. de Boer, A. K. Smilde, and D. A. Doornbos, Multicriteria decision making. Chemometrics and Intelligent Laboratory Systems, 16: 175-191 (1992).
29. A. K. Smilde, C. H. P. Bruins, and D. A. Doornbos, Optimization of the reversed-phase high-performance liquid chromatographic separation of synthetic estrogenic and progestogenic steroids using multicriteria decision making method, J. Chromatogr., 410: 1-12 (1987).
30. A. K. Smilde, A. Knevelman, and P. M. J. Coenegracht. Introduction of multicriteria descision making in optimization procedures for high-performance liquid chromatographic separations, J. Chromatogr., 369: 1-10 (1986).
31. R. Tijssen, P. J. Schoenmakers, M. R. Böhmer. L. K. Koopal, and H. A. H. Billiet, Lattice models for the description of partitioning/adsorption and retention in reversed-phase liquid chromatography, including surface and shape effects, J. Chromatogr., 656: 135-196 (1993).
32. C. Horváth, W. Melander, and I. Molnár, Solvophobic interactions in liquid chromatography with nonpolar stationary phases. J. Chromatogr., 125: 129-156 (1976).
33. C. Horváth and W. Melander, Liquid chromatography with hydrocarbonaceous bonded phases: Theory and practice of reversed phase chromatography. J. Chromatogr. Sci., 15: 393-404 (1977).
34. M. Otto, U. Hörchner, and W. Wegscheider, Multi-dimensional interpolation by the moving least-squares approach for modeling of chromatographic retention data. J. Chromatogr., 483: 453-460 (1989).
35. C. H. Bryant, A. Adam, D. R. Taylor, and R. C. Rowe. A review of expert systems for chromatography. Anal. Chim. Acta, 297: 317-34 (1994) 7.
36. T. Hamoir and D. L. Massart, Expert Systems in Chromatography, Advances in Chromatography, vol. 33, Marcel Dekker, New York, 1993, pp. 97-145.
37. B. Bourguignon, P. Vankeerberghen, and D. L. Massart, CRISEBOOK, a hypermedia version of an expert system for the selection of optimization criteria in high-performance liquid Chromatography, J. Chromatogr., 592: 51-57 (1992).
38. R. J. Laub and J. H. Purnell, Criteria for the use of mixed solvents in gas-liquid Chromatography, J. Chromatogr., 112: 71 (1975).
39. P. R. Haddad, A. C. J. H. Drouen, H. A. H. Billiet, and L. de Galan, Combined optimization of mobile phase pH and organic modifier content in the separation of some aromatic acids by reversed-phase HPLC, J. Chromatogr., 282: 71-81 (1983).
40. H. A. H. Billiet, J. Vuik, J. K. Strasters, and L. de Galan, Simultaneous optimization of reagent concentration and pH in reversed-phase ion-pairing Chromatography, J. Chromatogr., 384: 153-162 (1987).
41. A. C. J. H. Drouen, H. A. H. Billiet, and L. de Galan, A practical procedure for the optimization of reversed-phase separations with quaternary mobile phase mixtures, J. Chromatogr., 352: 127-139 (1986).
42. H. A. H. Billiet, C. Hendrikx-Jongerius, J. Frank, H. Corstjens, and K. Ch. A. M. Luyben, Optimization of gradient shape and composition in reversed-phase liquid chromatography. Lecture (1012-Th-L) at the 18th International Symposium on Column Liquid Chromatography, May 8-13, 1994, Minneapolis, MN, final program p. 170.
43. H. Corstjens, A. E. E. Oord, H. A. H. Billiet, J. Frank, and K. Ch. A. M. Luyben, Optimization of selectivity in capillary zone electrophoresis and micellar electrokinetic capillary chromatography using the iterative regression strategy, J. High Res. Chromatogr., 18: 551-557 (1995).
44. H. A. H. Billiet, P. E. Andersson, and P. R. Haddad, Computer optimization of background electrolyte composition in the separation of metal ions by capillary electrophoresis, Electrophoresis, 17: 1367-1372 (1996).
45. M. Mulholland, P. Preston, D. B. Hibbert, P. R. Haddad, P. Compton, Teaching a computer ion chromatography from a database of published methods. J. Chromatogr. A, , 755: 15-24 (1996).
46. M. Mulholland, K. McKinnon, P. R. Haddad. Practical evaluation of ion chromatography methods developed by an expert system. J. Chromatogr. A, 739: 25-33 (1996).
47. P. R. Haddad and P. E. Jackson, Ion Chromatography: Principles and Applications, Journal of Chromatography library, vol. 46, Elsevier, Amsterdam, 1990.
48. H. J. Metting and P. M. J. Coenegracht, Neural networks in high-performance liquid chromatography optimization: Response surface modeling, J. Chromatogr. A, 728: 47-53 (1996).
49. Y. L. Xie, J. J. Baeza-Baeza, J. R. Torres-Lapasió, M. C. Garcia-Alvarez-Coque, and G. Ramis-Ramos, Modeling and prediction of retention in high-performance liquid chromatography by using neural networks, Chromatographia, 41: 435-444 (1995).
50. A. Bartha, Gy. Vigh, H. A. H. Billiet, and L. de Galan. Studies in reversed-phase ion pair chromatography. Part 4. The role of the chain length of the pairing ion. J. Chromatogr., 303: 29-38 (1984).
51. A Bartha, Gy. Vigh, H. A. H. Billiet, and L. de Galan, Effect of the type of ion-pairing reagent in reversed-phase ion-pair chromatography, Chromatographia, 20: 587-590 (1985).
52. A. Bartha and Gy. Vigh, Studies in reversed-phase ion-pair chromatography. I. Adsorption isotherms of tetra alkylammonium ion-pair reagents on Lichrosorb RP-18 in methanol-water eluents. J. Chromatogr., 260: 337-345 (1983).
53. A. Bartha, H. A. H. Billiet, L. de Galan, and Gy. Vigh. Studies in reversed-phase ion-pair chromatography. Part 3. The effect of counter ion concentration. J. Chromatogr., 291: 91-102 (1984).
54. P. J. Schoenmakers, A. C. J. H. Drouen, H. A. H. Billiet, and L. de Galan, A simple procedure for the rapid optimization of RPLC-separations with ternary mobile phase mixtures. Chromatographia, 15: 688-696 (1982).
55. A. C. J. H. Drouen, H. A. H. Billiet, P. J. Schoenmakers, L. de Galan. An improved optimization procedure for the selection of mixed mobile phases in reversed-phase liquid chromatography. Chromatographia, 16: 48-52 (1982).
56. L. R. Snyder, J. W. Dolan, D. C. Lommen, DryLab computer simulation for high-performance liquid chromatographic method development. I. Isocratic elution. J. Chromatogr., 485: 65-89 (1989).
57. J. W. Dolan, D. C. Lommen, and L. R. Snyder, DryLab computer simulation for high-performance liquid chromatographic method development. II. Gradient elution. J. Chromatogr., 485: 91-112 (1989).
58. P. A. Bristow, J. H. Knox, Standardization of test conditions for high performance liquid chromatography columns, Chromatographia, 10: 279-289 (1977).
59. L. R. Snyder and J. W. Dolan, Initial experiments in high-performance liquid chromatographic method development. I. Use of a starting gradient run. J. Chromatogr. A, 721: 3-14 (1996).
60. J. A. Lewis, L. R. Snyder, and J. W. Dolan, Initial experiments in high-performance liquid chromatographic method development. II. Recommended approach and conditions for isocratic separation. J. Chromatogr. A, 721: 15-29 (1996).
61. R. F. Rekker, The Hydrophobic Fragmental Constant, Elsevier, Amsterdam, 1977.
62. T. Braumann, Determination of hydrophobic parameters by reversed-phase liquid chromatography: Theory, experimental techniques, and application in studies on quantitative structure-activity relationships. J. Chromatogr., 373: 191-225 (1986).
63. 0) based on the slope and intercept of the log k versus organic phase concentration plot. J. Chromatogr., 631: 49-61 (1993).
64. H. Engelhardt and M. Jungheim, Comparison and characterization of reversed-phases, Chromatographia, 29: 59-68 (1990).
65. P. Jandera and J. Churacek, Gradient Elution in Column Liquid Chromatography: Theory and Practice, Journal of Chromatography library, vol. 31, Elsevier, Amsterdam, 1985.
66. P. J. Schoenmakers, H. A. H. Billiet, R. Tijssen, and L. de Galan, Gradient selection in reversed-phase liquid chromatography. J. Chromatogr., 149: 519-537 (1978).
67. P. L. Zhu, L. R. Snyder, J. W. Dolan, N. M. Djordjevic, D. W. Hill, L. C. Sander, and T. J. Waeghe, Combined use of temperature and solvent strength in reversed-phase gradient elution. I. Predicting separation as a function of temperature and gradient conditions. J. Chromatogr. A, 756: 21-39 (1996).
68. P. L. Zhu, J. W. Dolan, L. R. Snyder, Combined use of temperature and solvent strength in reversed-phase gradient elution. II. Comparing selectivity for different samples and systems. J. Chromatogr., 756: 41-50 (1996).
69. L. R. Snyder in K. Gooding and F. E. Regnier (eds.), HPLC of Biological Macromolecules: Methods and Applications, chromatographic Science, vol. 51. Dekker, New York, 1990.
70. S. Heinisch and J. L. Rocca, Optimization of a multisolvent composition in RPHPLC: Generalization to non-ideal peaks. Chromatographia, 41: 544-552 (1995).
71. S. Heinisch, P. Riviere, and J. L. Rocca, Computerized optimization of gradient elution conditions with ternary solvent mobile phases in RPLC, Chromatographia, 39: 216-223 (1994).
72. S. Heinisch, J. L. Rocca, and M. Kolosky, Computerized optimization of the mobile phase composition in gradient elution reversed-phase HPLC. Chromatographia, 29: 482-488 (1990).
73. S. V. Galushko and A. A. Kamenchuk, Total search: Superfast computer-aided method for optimizing multisegment gradient profile. Poster We/Th P-487/2 at HPLC'95, Innsbruck, Austria.
74. S. V. Galushko and A. A. Kamenchuk. Fast optimization of the multi-segment gradient profile in reversed-phase high performance liquid chromatography using the Monte-Carlo method. LC-GC International, 8: 581 (1995).
75. G. Rippel, unpublished results.
76. P. J. Schoenmakers, H. A. H. Billiet, and L. de Galan, Influence of organic modifiers on the retention behavior in reversed-phase liquid chromatography and its consequences for gradient elution. J. Chromatogr., 185: 179-195 (1979).