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A part of this work has been orally reported at the 227 ACS National Meeting in Anaheim, CA. March 28, 2004.
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Compound 2a has been obtained as a by product, and its X-ray structure has been reported. However, there is no procedure for the formation of 2a. See: Rheingold, A. L.; Staley, D. L.; Heck, R. F.; Silverberg, L. Acta Crystallogr. 1990, C46, 144-146.
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33645590617
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note
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4, (0.05 mmol). After stirring the mixture at 50 °C for 24 h, 4 was obtained.
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