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The Kugelrohr tubes (three bulbs) are handmade from 10-mm pyrex glass tubing. Samples are recovered by breaking the tubes on each side of the bubble containing the distillate. If making tubes is a problem, any micro-distillation apparatus could likely be substituted. A Kugelrohr distillation apparatus has been described: Reasonably small Kugelrohr bulbs are available commercially (Chemglass, Inc.)
-
The Kugelrohr tubes (three bulbs) are handmade from 10-mm pyrex glass tubing. Samples are recovered by breaking the tubes on each side of the bubble containing the distillate. If making tubes is a problem, any micro-distillation apparatus could likely be substituted. A Kugelrohr distillation apparatus has been described: Graeve, R.; Wahl, G., Jr. J. Chem. Educ. 1964, 41, 279. Reasonably small Kugelrohr bulbs are available commercially (Chemglass, Inc.).
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Wahl Jr., G.2
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