Standardization of crude extract of neem seed kernels (Azadirachta indica A. Juss) and commercial neem based formulations using HPTLC and extended length packed-columns SFC method

Chromatographia

Volumn 62, Issue 3-4, 2005, Pages 183-195

  Agrawal, H ^a   Kaul, N ^a   Paradkar, A R ^a   Mahadik, K R ^a  

^a BHARATI VIDYAPEETH DEEMED UNIVERSITY   (India)

Author keywords

Azadirachtin A and B; Neem seed kernels; Salannin and nimbin; Supercritical fluid chromatography; Thin layer chromatography

Indexed keywords

ACETIC ACID ETHYL ESTER; AZADIRACHTA INDICA EXTRACT; AZADIRACHTIN A; AZADIRACHTIN B; BENZENE; CARBON DIOXIDE; METHANOL; NIMBIN; SALANNIN; SILICA GEL; UNCLASSIFIED DRUG;

ANALYSIS OF VARIANCE; ANALYTICAL EQUIPMENT; ARTICLE; CORRELATION ANALYSIS; DIODE; DRUG DETERMINATION; DRUG FORMULATION; FLOW RATE; HIGH PERFORMANCE THIN LAYER CHROMATOGRAPHY; PLANT SEED; PRIORITY JOURNAL; SEPARATION TECHNIQUE; STANDARDIZATION; STUDENT T TEST; SUPERCRITICAL FLUID CHROMATOGRAPHY;

EID: 23844479589     PISSN: 00095893     EISSN: None     Source Type: Journal    
DOI: 10.1365/s10337-005-0588-6     Document Type: Article

References (61)

1. Butterworth JH, Morgan ED (1968) J Chem Soc Chem Commun 23-24
2. Butterworth JH, Morgan ED (1972) J Insect Physiol 17:969-977
3. Broughton HB, Ley SV, Slawin AMZ, Williams DJ, Morgan ED (1986) J Chem Soc Chem Commun 46-50
4. Kraus W, Bokel M, Klenk A, Pohnl H (1985) Tetrahedron Lett 26:6435-6436
5. Jacobson M, Green MB, Hedin PA (1986) ACS Symposium Series, American Chemical Society, Washington, DC, 269:220-222
6. Mordue AJ, Blackwell A (1993) J Insect Physiol 39:903-924
7. Schmutterer H (1995) Insecta, Insects in the Neem Tree (H. Schmutterer, ed.) VCH, Weinheim, 167-365
8. Harris M, Henderson R, McCrindle M, Overton KH, D. W. Turner (1968) Tetrahedron 24:1517-1523
9. Warthen JD, Uebel EC, Dutky SR, Lusby WR, Feingold H (1978) Agric Res Results, (North eastern Ser.) ARR-NE-2
10. Warthen JD, Stokes JB, Jacobson M, Kozempel MF (1984) J Liq Chromatogr 7:591-595
11. Yamasaki RB, Klocke JA, Lee SM, Stone GA, Darlington MV (1986) J Chromatogr 356:220-226
12. Thejavathi R, Shirish R, Yakkundi S, Ravindranath B (1995) J Chromatogr A 705:374-379
13. Kaushik N (2002) Anal Bioanal Chem 374:1199-1204
14. Barrek S, Paisse O, Grenier-Loustalot MF (2004) Anal Bioanal Chem 378:753-763
15. Schaaf O, Jarvis AP, van der Esch SA, Giagnacovo G, Oldham NJ (2000) J Chromatogr A 886:89-97
16. Vuorela P, Rahko EL, Hiltunen R, Vuorela H (1994) J Chromatogr A 670:191-198
17. Ferenczi-Fodor K, Vigh Z, Nagy-Turak A, Renger B, Zeller M (2001) J AOAC Int 84:1265-1276
18. Ferenczi-Fodor K, Vigh Z (2001) Planar Chromatography - A Retrospective View from the Third Millennium (Sz. Nyiredy, ed.), Springer Scientific Publisher, Budapest, 336-352
19. rd edn 1998, Suppl., pp. 5-7
20. Thin layer chromatography (2002) Monograph 2.2.27, European Pharmacopoeia, Published by Council of Europe 4.5:3638-3642
21. Mantovani G, Vaccari G, Dosi E, Lodi G (1998) Carbohydr Polym 37:263-269
22. Doner LW (2001) Chromatographia 53:579-583
23. nd edn pp. 129-148 and pp. 273-306
24. Renger B (1993) J AOAC Int 76:7-14
25. Abdelrahman AN, Karim EIA, Ibrahim KEE (1994) J Pharm Biomed Anal 12:205-208
26. Kaniou I, Zachariadis G, Kalligas G, Tsoukali H, Stratis J (1994) J Liq Chromatogr 17:1385-1398
27. Ponder GW, Stewart JT (1994) J Chromatogr A 659:177-183
28. Weins C, Hauck HE (1996) LC GC 14:456-464
29. McCarthy KE, Wang Q, Tsai EW, Gilbert RE, Brooks MA (1998) J Pharm Biomed Anal 17:671-677
30. Jovanovic SE, Agbaba D, Zivanov-Stakic D, Vladimirov S (1998) J Pharm Biomed Anal 18:893-898
31. WHO, Guidelines for the Assessment of Herbal Medicine, Munich, World Health Organization, 1991
32. Küppers S, Lorenschaft B, Schmitz FP, Klesper E (1989) J Chromatogr 475:85-94
33. Schmitz FP, Klesper E (1990) J Supercrit Fluids 3:29-34
34. van Puyvelde F, van Rompay P, Chimowitz EH (1992) J Supercrit Fluids 5:227-232
35. Linnemann KH, Wilsch A, Schneider GM (1986) J Chromatogr 369:39-42
36. Gyllenhaal O, Vessman J (1993) J Chromatogr 628:275-280
37. Petersson P, Lundell N, Markides KE (1992) J Chromatogr 623:129-134
38. Jenkins TJ, Kaplan M, Simmonds MR (1991) Analyst 116:1305-1308
39. Bhoir IC, Sundaresan M, Bhagwat AM (1997) Anal Chim Acta 354:123-128
40. Patel YP, Sundaresan M, Bhagwat AM, Raman B (1997) Indian J Pharm Sci 59:3-8
41. Patil ST, Sundaresan M, Bhoir IC, Bhagwat AM (1998) Talanta 47:3-10
42. Bhoir SI, Sundaresan M, Bhoir IC, Bhagwat AM (2001) J Chromatogr B 757:39-47
43. Bari VR, Dhorda UJ, Sundaresan M (1997) Talanta 45:297-304
44. Bhoir IC, Sundaresan M, Bhagwat AM, Raman B (1998) J Pharm Biomed Anal 17:539-546
45. Bari VR, Sundaresan M, Dhorda UJ (1998) Anal Chim Acta 376:221-225
46. Patil ST, Sundaresan M, Bhoir IC (1999) Talanta 48:1179-1189
47. Bhoir IC, Raman B, Sundaresan M, Bhagwat AM (1997) Anal Chim Acta 354:123-132
48. Patil ST, Sundaresan M, Bhoir IC (1999) Anal Chim Acta 384:143-150
49. Simmons BR, Jagota NK, Stewart JT (1994) J Pharm Biomed Anal 12:1317-1323
50. Smith MS, Oxford J, Evans MB (1994) J Chromatogr 683:402-406
51. Strode JTB, Taylor LT, Howard AL, Brooks MA (1994) J Pharm Biomed Anal 12:1003-1009
52. Mount DL, Todd GD, Navaratnam V (1995) J Chromatogr 666:183-187
53. Patel YP, Sundaresan M, Dhorda UJ (1998) Talanta 47:625-630
54. Berger TA, Wilson WH (1993) Anal Chem 65:1451-1455
55. ICH, Q2A Validation of Analytical Procedure: Methodology, International Conference on Harmonization, Geneva, October, 1994
56. ICH, Q2B Validation of Analytical Procedure: Methodology, International Conference on Harmonization, Geneva, March, 1996
57. ICH Guidance on Analytical Method Validation, International Convention on Quality for the Pharmaceutical Industry, Toronto, Canada, September 2002
58. McCarthy KE, Wang Q, Tsai EW, Gilbert RE, Brooks MA (1998) J Pharm Biomed Anal 17:671-677
59. Fried B, Sherma J (1994) Thin-Layer Chromatography, Techniques and Applications, third edn Marcel Dekker, New York
60. Sethi PD (1996) High Performance Thin Layer Chromatography, Quantitative Analysis of Pharmaceutical Formulations, CBS Publishers and Distributors, New Delhi
61. Miller JC, Miller JN (1992) Statistics for Analytical Chemistry, second ed., Ellis Horwood, New York