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3: C, 47.08; H, 4.25; N, 8.45. Found: C, 47.25; H, 4.33; N, 8.26.
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43
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note
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3. A total of 20256 reflections up to θ = 28.30 were collected, of which 15698 unique reflections were used. The structure was solved using SHELXS-97 and refined using SHELXL-97 to R1 = 0.0429, wR2 = 0.1072, and GOF = 1.051. All non-hydrogen atoms were refined anisotropically. Hydrogen atoms were located in successive difference Fourier maps, and they were treated as riding atoms using SHELXL default parameters.
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See the Supporting Information
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See the Supporting Information.
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