Exploring uncharted terrain in nature's structure space using capillary NMR spectroscopy: 13 Steroids from 50 fireflies

Journal of the American Chemical Society

Volumn 127, Issue 31, 2005, Pages 10810-10811

  Gronquist, Matthew ^a   Meinwald, Jerrold ^b   Eisner, Thomas ^b   Schroeder, Frank C ^b  

^a STATE UNIVERSITY OF NEW YORK   (United States)

^b Department of Population Medicine and Diagnostic Sciences   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

LUCIBUFAGIN; NATURAL PRODUCT; PYRONE DERIVATIVE; STEROID; SUCROSE; UNCLASSIFIED DRUG;

ARTHROPOD; ARTICLE; CHEMICAL STRUCTURE; CONTROLLED STUDY; HEMOLYMPH; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LUCIDOTA ATRA; MAGNETIC FIELD; NONHUMAN; NUCLEAR OVERHAUSER EFFECT; PREDATOR; PROTON NUCLEAR MAGNETIC RESONANCE; SIGNAL NOISE RATIO; STRUCTURE ANALYSIS;

ANIMALS; BEETLES; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MAGNETIC RESONANCE SPECTROSCOPY; STEROIDS;

EID: 23744504882     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja053617v     Document Type: Article

References (9)

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8. For a comparison of CapNMR and 5 mm HCN probe with Shigemi tube using a 17.2 μg sucrose sample, see Supporting Information.
9. For a detailed description of sample preparation for CapNMR analysis, see Supporting Information.