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note
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2 (0.60 mmol, 53.42 mg). After stirred for another 5 min, the solution was filtered and the filtrate was slowly evaporated in air. After two weeks, red block crystals of complex 1 were isolated. Yield 65%. Green block crystals of complex 2 were prepared in a similar manner to those of complex 1. Yield 57%. Satisfied elemental analysis was obtained for each complex
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17
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33646661599
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note
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2 using SHELXL-97 program. All non-H atoms were refined anisotropically, the H atoms attached to C atoms were added at calculated position with C-H distances 0.96-0.97 Å. CCDC 227601-227602 (for 1 and 2, respectively) contain the supplementary crystallographic data for this paper
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