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1H resonances upfield of -20 ppm are not decoupled.
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2342442911
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note
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The catalyst contains 34 exchangeable hydrogen atoms in each molecule.
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2342420691
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It is possible that β-hydride elimination, if it occurs by dechelation of the drape ligand, would form a species with coordinated HNCO. If this is the case, and the hydrides maintained their inequivalence, scrambling of the deuterium label might not be observed.
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