Crystal structure of (2S,7R)-N-benzhydryl-2-(1′-hydroxyethyl)-6-phenyl-5,6-dehydromorpholin-3-one, C25H23NO3

Zeitschrift fur Kristallographie - New Crystal Structures

Volumn 216, Issue 1-4, 2001, Pages 51-52

  Tinant, B ^a   Declercq, J P ^a   Ceresiat M ^b   Marchand Brynaert, J ^a  

^a UNIVERSITÉ CATHOLIQUE DE LOUVAIN   (Belgium)

^b Tessenderlo Chemie   (Belgium)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 23044527363     PISSN: 14337266     EISSN: None     Source Type: Journal    
DOI: 10.1524/ncrs.2001.216.14.51     Document Type: Article

References (14)

1. Berks, A. H.: Preparation of Two Pivotal Intermediates for the Synthesis of 1 -β-Methy 1 Carbapenem Antibiotics. Tetrahedron 52 (1996) 331-375.
2. Hanessian, S.; Bedeschi, A.; Battistini, C.; Mongelli, N.: A New Synthetic Strategy for the Penems. Total Synthesis of (5R,6S,8R)-6-(a-Hydroxy-ethyl)-2-(hydroxymethyl) Penem-3-carboxylic Acid. J. Am. Chem. Soc. 107(1985) 1438-1439.
3. Maruyama, H.; Shiozaki, M.; Hiraoka, T.: A Synthesis of a Versatile Intermediate Leading to Thienamycin Analogs. Bull. Chem. Soc. Jpn. 58 (1985) 3264-3270.
4. Chackalamannil, S.; Fett, N.; Kirkup, M.; Afonso, A.; Ganguly, A. K.: An Efficient Synthesis of (3R,4R)-3-(l-(R)-Hydroxyethyl)-4-(benzoyl-oxy)-2-azetidinone from L-Threonine. Use of Phenylalkoxymethyl as a Novel N-Protecting Group. J. Org. Chem. 53 (1988) 450-452.
5. Kugelman, M.; Gala, D.; Jaret, R. S.; Nyce, P. L.; McPhail, A. T.: Synthesis of Azetidinones from L-Threonine : Formation of Unusually Stable Bicyclic Hemi-ketals and cis-Azetidinones. Synlett (1990) 431-432.
6. Demillequand, M.; Cérésiat, M.; Belmans, M.; Kemps, L.; Marchand-Brynaert, J.: Analytical Separation of the Four Stereoisomers of Isopropy1 2,3-Epoxybutanoate by Gas Chromatography. J. Chromatography A832 (1999) 259-264.
7. Deng, B.-L.; Demillequand, M.; Laurent, M.; Touillaux, R.; Belmans, M.; Kemps, L.; Cérésiat, M.; Marchand-Brynaert, J.: Preparation of (3S, 45)-1 -benzhydryl-3-[(5R)-1′-hydroxyethyl]-4-acyl-2-azetidinones from (2R, 3R)-epoxybutyramide Precursors. Tetrahedron 56 (2000) 3209-3217.
8. Marchand-Brynaert, J.; Moya-Portuguez, M.; Lesuisse, D.; Ghosez, L.: 2-Amino-l-azetines, a New Class of Strained Amidines. J. Chem. Soc. Chem. Commun. (1980) 173-174.
9. Duax, W. L.; Weeks, C. M.; Rohrer, D. C.: Topics in Stereochemistry, Vol. 9(1976) 271-383.
10. Cremer, D.; Pople, J. A.: General definition of ring puckering coordinates. J. Am. Chem. Soc. 97 (1975) 1354-1358.
11. Otwinoswski, Z. and Minor, W. (1997) Methods in Enzymology, Vol. 276, p. 307-326. Edts. C. W. Carter, Jr. and R. M. Sweet, Academic Press.
12. Sheldrick, G. M.: Phase Annealing in SHELX-90: Direct Methods for Larger Structures. Acta Crystallogr. A46 (1990) 467-473.
13. Sheldrick, G. M.: SHELXL-93 Program for the Refinement of Crystal Structures. University of Göttingen, Germany 1993.
14. Spek, A. L.: PLATON, Molecular Geometry Program. University of Utrecht, The Nederlands 1998.