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note
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Reaction vessel description: The reaction vessel was fabricated as a 100 mL three-neck U-bottom flask with the right and left necks being #7 Chem-Thread adaptors from chemglass and the middle neck as a 19/38 Wheaton Clear Seal female adaptor. A reflux condenser is connected to the reaction flask with the male 19/38 Wheaton Clear Seal adaptor, and the condenser top is a 24/40 ground glass adaptor. A glass thermometer holder is placed in the right #7 Chem-Thread adaptor, while a rubber septum is placed in the other #7 Chem-Thread adaptor.
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note
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