Direct chiral separation of N-fluorenylmethoxycarbonyl α-amino acids by HPLC for determination of enantiomeric purity

Bulletin of the Korean Chemical Society

Volumn 26, Issue 6, 2005, Pages 998-1000

  Yin, Hua Li ^a   Baek, Chae Sun ^a   Byung, Wook Jo ^a   Lee, Wonjae ^a  

^a Chosun University   (South Korea)

Author keywords

Chiral stationary phase; Enantiomer separation; N FMOC amino acids

Indexed keywords

EID: 22744437991     PISSN: 02532964     EISSN: None     Source Type: Journal    
DOI: 10.5012/bkcs.2005.26.6.998     Document Type: Article

References (18)

1. Greene, T. W.; Wuts, P. G. M. Protective Groups in Organic Synthesis, 3rd Ed.; John Wiley & Sons. Inc.: New York, 1999.
2. Einarsson, S.; Folestad, S.; Josefsson, B.; Lagerkvist, S. Anal. Chem. 1986, 58, 1638.
3. Brückner, H.; Lüpke, M. J. Chromatogr. A 1996, 697, 295.
4. Burgess, K. Solid-Phase Organic Synthesis, 3rd Ed.; John Wiley & Sons. Inc.: New York, 2000.
5. Jung, G. Combinatorial Chemistry: Synthesis, Analysis, Screening; Wiley-VCH: Tubingen, 1999.
6. Zukowski, J.; Pawlowska, M.; Armstrong, D. W. J. Chromatogr. 1992, 623, 33.
7. Tang, Y.; Zukowski, J.; Armstrong, D. W. J. Chromatogr. A 1996, 743, 261.
8. Ekborg-Ott, K. H.; Liu, Y.; Armstrong, D. W. Chirality 1998, 10, 434.
9. Piccinini, A.-M.; Schmid, M. G.; Pajpanova, T.; Pancheva, S.; Grueva, E.; Gubitz, G. J. Biochem. Biophys. Methods 2004, 61, 11.
10. Oi, H.; Kitahara, H.; Aoki, F.; Kisu, N. J. Chromatogr. A 1995, 689, 195.
11. Pirkle, W. H.; Lee, W. Bull. Korean Chem. Soc. 1998, 19, 1277.
12. Krawinkler, K. H.; Maier, N. M.; Sajovic, E.; Lindner, W. J. Chromatogr. A 2004, 1053, 119.
13. Knoche, B.; Milosavljev, S.; Gropper, S.; Brunner, L. A.; Powell, M. L. J. Chromatogr. B 1997, 695, 355.
14. Application guide for chiral HPLC selection, third Edition, Daicel Chemical Industries, Ltd.
15. Kim, B.-H.; Lee, W. J. Liq. Chromatogr. & Rel. Tech. 1999, 22, 523.
16. Lee, W.; Kim, B.-H. J. High Resol. Chromatogr. 1998, 21, 189.
17. Bodansky, M.; Bodansky, A. The Practice of Peptide Synthesis; Springer: New York, 1984.
18. Perry, J. A.; Rateike, J. D.; Szczerba, T. J. J. Chromatogr. 1987, 389, 57.