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see Ref. 8a
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n ratio of 6a, see Ref. 8a.
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22244470133
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31PNMR data were obtained by monitoring the reaction mixtures, indicating complex formation. Signals due to the terminal moieties were not detected because of low concentration due to poor solubility of 6. After working up, the complexes were hardly soluble in common organic solvents.
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