Hydrothermal synthesis, crystal structures, and magnetic properties of a novel three-dimensional iron phosphite: NH4·Fe 2IIFeIII(HPO3)4]

Inorganic Chemistry Communication

Volumn 8, Issue 8, 2005, Pages 661-664

  Fan, Yong ^a   Song, Tianyou ^a   Li, Guanghua ^a   Shi, Zhan ^a   Yu, Guanghui ^a   Xu, Jianing ^a   Feng, Shouhua ^a  

^a JILIN UNIVERSITY   (China)

Author keywords

3D framework; Anti ferromagnetic; Hydrothermal synthesis; Iron phosphite

Indexed keywords

EID: 22044441625     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2005.04.012     Document Type: Article

References (16)

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16. 2 = 0.0663. The intensity data were collected on a Siemens SMART CCD diffractometer with graphite-monochromated Mo Kα (λ = 0.71073 Å) radiation at 293 K. Data were processed on a PC with the SAINT processing program. The structures were solved by direct methods using the SHELXTL crystallographic software package. The iron and phosphorus atoms were located first, while the nitrogen, and oxygen atoms were found in the difference Fourier maps. The hydrogen atoms on the amine molecules were calculated, while the hydrogen atoms on the phosphites were located (ICSD number 414407).