Planarity of N′-(amino-2-pyridylmethylene)-hydrazide carbodithioic acid frame and crystal structure of its methyl ester dihydrate

Journal of Chemical Crystallography

Volumn 35, Issue 6, 2005, Pages 477-480

  Główka, Marek L ^a   Martynowski, Dariusz ^a   Olczak, Andrzej ^a   Orlewska, Czesława ^b   Foks, Henryk ^b   Bojarska, Joanna ^a   Szczesio, Małgorzata ^a   Gołka, Jolanta ^a  

^a LODZ UNIVERSITY OF TECHNOLOGY   (Poland)

^b MEDICAL UNIVERSITY OF GDANSK   (Poland)

Author keywords

Crystal structure; Dipolar form; Flat non aromatic molecule; intramolecular hydrogen bonds; Six bonds conjugation; Thiolate ester

Indexed keywords

(1 METHYL 2 PYRROLIDINYLIDENE)HYDRAZINECARBODITHIOIC ACID METHYL ESTER; HYDRAZIDE DERIVATIVE; N' (AMINO 2 PYRIDYLMETHYLENE)HYDRAZIDE CARBODITHIOIC ACID; NITROGEN; SOLVENT; SULFUR; UNCLASSIFIED DRUG;

ARTICLE; CONFORMATION; CONJUGATION; CRYSTAL STRUCTURE; DIPOLE; DONOR; FRAGMENTATION REACTION; HYDROGEN BOND; SPACE;

EID: 21644437628     PISSN: 10741542     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10870-005-2360-z     Document Type: Article

References (9)

1. Foks, H.; Orlewska, C. Acta Polon. Pharm. Drug Res. 1992, 49, 47-52.
2. Mamolo, M.G.; Vio, L.; Banfi, E.; Cinco, M. Eur. J. Med. Chem. Chim. Ther. 1986, 21, 467-474.
3. Orlewska, C.; Foks, H.; Sowiński, P.; Martynowski, D.; Olczak, A.; Główka, M.L. Polish J. Chem. 2001, 75, 1237-1245.
4. KM-4 Manual, KUMA Diffraction: Wrocław, Poland, 1992.
5. Sheldrick, G.M. SHELXTL/PC, Version 4.1, An integrated System for Solving, Refining and Displaying Crystal Structures from Diffraction Data, Siemens Analytical X-Ray Instruments; Inc. Medison: Wisconsin, USA, 1990.
6. Sheldrick, G.M. SHELXL97, Program for Refinement of Crystal Structures; University of Göttingen: Germany, 1997.
7. Radics, U.; Liebscher, J.; Ziemer, B.; Rybakov, V. Chem. Ber. 1992, 125, 1389-1395.
8. Główka, M.L.; Martynowski, D.; Olczak, A.; Kozłowska, K.; Ołubek, Z.; Orlewska, C.; Foks, H. Polish J. Chem. 1999, 73, 845-851.
9. Spek, A.L. PLATON, A Multipurpose Crystallographic Tool; Utrecht University: The Netherlands, 2003.