Quantification in capillary electrophoresis-mass spectrometry: Long- and short-term variance components and their compensation using internal standards

Electrophoresis

Volumn 26, Issue 12, 2005, Pages 2360-2375

  Ohnesorge, Jens ^a   Sänger van de Griend, Cari ^b   Wätzig, Hermann ^a  

^a TECHNICAL UNIVERSITY OF BRAUNSCHWEIG   (Germany)

^b ASTRAZENECA R AND D   (Sweden)

Author keywords

Capillary electrophoresis mass spectrometry; Electrospray; Isotopically labelled internal standard; Precision; Quantitation; Validation

Indexed keywords

CAPILLARY ELECTROPHORESIS; DRUG PRODUCTS; ELECTROSPRAY IONIZATION;

CAPILLARY ELECTROPHORESIS-MASS SPECTROMETRIES; ELECTROSPRAYS; INTERNAL STANDARDS; ISOTOPICALLY LABELLED INTERNAL STANDARDS; PEAKS AREAS; PRECISION; QUANTITATION; RELATIVE STANDARDS DEVIATIONS; REPRODUCIBILITIES; VALIDATION;

MASS SPECTROMETRY;

2 PROPANOL; AMMONIUM ACETATE; BUFFER; NEOSTIGMINE; NICOTINIC ACID; PARACETAMOL; SCOPOLAMINE BROMIDE;

ARTICLE; CALCULATION; CAPILLARY ELECTROPHORESIS; CONCENTRATION RESPONSE; DRUG DETERMINATION; ELECTROSPRAY; MASS SPECTROMETRY; PH; QUANTITATIVE ANALYSIS; SIGNAL NOISE RATIO; STANDARD; ULTRAVIOLET RADIATION; VALIDATION PROCESS;

EID: 21644437195     PISSN: 01730835     EISSN: None     Source Type: Journal    
DOI: 10.1002/elps.200410413     Document Type: Article

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