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21644445710
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note
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2)(all data) = 0.084 for 2665 unique reflections. All the hydrogen atoms were found experimentally. Appreciable electron densities were observed in a hexagonal channel and tentatively assigned as oxygen atoms. CCDC No. 250464.
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12
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21644482531
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note
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9 Symmetry operation codes. *) 2/3 - x, 1/3 - y, 4/3 - z. #) 2/3 - y, 1/3 + x - y, 1/3 + z. †) 1/3 - x + y, 2/3 - x, -1/3 + z. §) x - y, x, 1 - z. ‡) -1/3 + y, 1/3 - x + y, 4/3 - z.
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13
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21644455158
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note
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molT value between 50-100 K exhibited significant sample-dependence, probably due to absorbed oxygen.
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19
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21644484867
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note
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14): C, 27.09; H, 3.91; N, 21.06%. Found: C, 26.47; H, 3.98; N, 20.20%. After being pumped: Anal. Found: C, 25.78; H, 3.52; N, 20.57%.
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