Isolation of two sucrose esters from Polygala tenuifolia by high speed countercurrent chromatography

Journal of Liquid Chromatography and Related Technologies

Volumn 28, Issue 10, 2005, Pages 1583-1592

  Jiang, Yong ^a   Tu, Pengfei ^a   Chen, Xiaojia ^a   Zhang, Tianyou ^b  

^a PEKING UNIVERSITY HEALTH SCIENCE CENTER   (China)

^b Beijing Inst New Technol Applic   (China)

Author keywords

3,6 Disinapoyl sucrose; High speed countercurrent chromatography; Polygala tenuiflolia; Tenuifoliside A

Indexed keywords

CHROMATOGRAPHY; ETHANOL; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH SPEED PHOTOGRAPHY; NUCLEAR MAGNETIC RESONANCE; SOLVENTS; SUGAR (SUCROSE); WATER;

BUTANOL; CORTEXES; CRUDE FRACTION; SOLVENT SYSTEMS; SUCROSE ESTERS;

ESTERS;

3,6' DISINAPOYL SUCROSE; CHLOROFORM; METHANOL; SUCROSE ESTER DERIVATIVE; TENUIFOLISIDE; UNCLASSIFIED DRUG; WATER;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH SPEED COUNTERCURRENT CHROMATOGRAPHY; INFRARED SPECTROMETRY; MASS SPECTROMETRY; PROTEIN ISOLATION; PROTEIN STRUCTURE; PROTON NUCLEAR MAGNETIC RESONANCE;

POLYGALA; POLYGALA TENUIFOLIA;

EID: 20844452735     PISSN: 10826076     EISSN: None     Source Type: Journal    
DOI: 10.1081/JLC-200058371     Document Type: Article

References (14)

1. Jiangsu New Medicinal College Dictionary of Chinese Drugs; Shanghai Scientific Technologic Publisher: Shanghai, 1997; 2174.
2. Sakuma, S.; Shoji, J. Studies on the Constituents of the Root of Polygala tenuifolia Willdenow. I. Isolation of Saponins and Structures of Onjisaponins G and F. Chem. Pharm. Bull. 1981, 21 (9), 2431-2441.
3. Fujita, T.; Liu, D.Y.; Ueda, S.; Takeda, Y. Xanthones from Polygala tenuifolia. Phytochemistry 1992, 31 (11), 3997-4000.
4. Ikeya, Y.; Sugama, K.; Okada, M.; Mitsuhashi, H. Four New Phenolic Glycosides from Polygala tenuifolia. Chem. Pharm. Bull. 1991, 39 (10), 2600-2605.
5. Jiang, Y.; Tu, P.F. Four Xanthone O-glycosides from Polygala tenuifolia. Phytochemistry 2002, 60 (8), 813-816.
6. Susumu, I.; Atsushi, I.; Takuji, Y.; Yukinobu, I. Brain Functional Improver. JP Patent 7179348A, July 18, 1995.
7. Ikeya, Y.; Takeda, S.; Tunakawa, M.; Karakida, H.; Toda, K.; Yamaguchi, T.; Aburada, M. Cognitive Improving and Cerebral Protective Effects of Acylated Oligosaccharides in Polygala tenuifolia. Bio. & Pharm. Bull. 2004, 27 (7), 1081-1085.
8. Miyase, T.; Ueno, A. Sucrose Derivatives from the Roots of Polygala tenuifolia. Shoyakugaku Zasshi 1993, 47 (3), 267-276.
9. Ito, Y. High speed Countercurrent Chromatography. CRC Crit. Rev. Anal. Chem. 1986, 17, 65-75.
10. Zhang, T.Y.; Pannell, L.K.; Pu, Q.L. Separation of Hydroxyanthraquinone Derivatives Extracted from Rheum with Analytical High Speed Countercurrent Chromatography. J. Chromatogr. A 1988, 442, 455-458.
11. Zhang, T.Y.; Xiao, R.; Xiao, Z.Y.; Pannell, L.K.; Ito, Y. Rapid Separation of Flavanoids by Analytical High Speed Countercurrent Chromatography. J. Chromatogr. A 1988, 445, 199-206.
12. Degenhardt, A.; Habben, S.; Winterhalter, P. Isolation of the Lignan Secoisolariciresinol Diglucoside from Flaxseed (Linum usitatissimum L.) by High Speed Countercurrent Chromatography. J. Chromatogr. A 2002, 943, 299-302.
13. Miyase, T.; Yamamoto, R.; Ueno, A. Phenylethanoid Glycosides from Stachys officinalis. Phytochemistry 1996, 43 (2), 475-479.
14. Oshikawa, M.; Murakami, T.; Matsuda, H.; Ueno, T.; Kadoya, M.; Yamahara, J.; Murakami, N. Bioactive Saponins and Glucosides. II. Senegae Radix. (2): Chemical Structures, Hypoglyceric Activity, and Ethanol Absorption Inhibitory Effect of E-senegasaponin c, Z-senegasaponin c, and Z-senegins II, III, and IV. Chem. Pharm. Bull. 1996, 44 (7), 1305-1313.