Synthesis and crystal structure of unprecedented oxo/hydroxo-bridged polynuclear gallium(III) aqua complexes

Inorganic Chemistry

Volumn 44, Issue 12, 2005, Pages 4133-4135

  Gerasko, Olga A ^a   Mainicheva, Ekaterina A ^a   Naumov, Dmitry Yu ^a   Kuratieva, Natalia V ^a   Sokolov, Maxim N ^a   Fedin, Vladimir P ^a  

^a NIKOLAEV INSTITUTE OF INORGANIC CHEMISTRY   (Russian Federation)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 20744454739     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic0502271     Document Type: Article

References (29)

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21. max = 0.5258/0.7185. The data collection for 1-3 was performed on a Bruker Nonius X8Apex diffractometer (Mo Kα., λ = 0.71073 Å) equipped with a CCD area detector. The structures were solved by direct methods and refined by the full-matrix least-squares method (Sheldrick, G. M. SHELXTL, version 6.12; Bruker-AXS, Inc.: Madison, WI, 2004).
22. Ahman, J.; Svensson, G.; Albertsson, J. Acta Crystallogr. 1996, C52, 1336-1338.
23. (a) Johansson, G. Ark. Kemi 1963, 20, 305-319.
24. (b) Johansson, G. Ark. Kemi 1963, 20, 321-342.
25. max = 0.4875/0.5189.
26. 40: C, 27.11; H, 4.68; N, 23.71. Found: C, 27.30; H, 4.78; N, 23.81.
27. max = 0.8620/0.9198.
28. 2O was described recently: Rather, E.; Gatlin, J. T.; Nixon, P. G.; Tsukamoto, T.; Kravtsov, V.; Johnson, D. W. J. Am. Chem. Soc. 2005, 127, 3242-3243.
29. 3+ in aqueous solution at pH 1.6 and 1.8.