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We could not completely separate two kinds of crystalline materials. Therefore, the yield was not shown.
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20444476097
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note
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-1): 3430 bm, 3121 w, 2473 w, 2352 w, 2165 w, 2103 w, 1952 w, 1641 m, 1606 m, 1586 s, 1567 m, 1492 m, 1475 w, 1420 m, 1414 s, 1322 w, 1238 m, 1224 m, 1192 w, 1167 w, 1121 m, 1091 m, 1052 m, 1027 m, 1018 m, 990 w, 979 w, 965 w, 839 s, 736 w, 567 s, 558 s, 527 w, 520m.
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43
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20444474482
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note
-
2O molecule were intricately disordered. Therefore, the hydrogen-bonding distances were not shown.
-
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44
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20444433093
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note
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The size was measured by considering van der Waals radii for constituting atoms. Hereafter, all size estimations of pores were made in this way.
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45
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0001792356
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50
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20444488334
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note
-
With one exception, the intramolecular dihedral angle of the type C azpy ligand in 1 was large (26Z°). This is probably because the molecular structure of the type C azpy ligand is disordered.
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