An in situ time-resolved XRD-PSD investigation into Na-montmorillonite interlayer and particle rearrangement during dehydration

Clays and Clay Minerals

Volumn 52, Issue 2, 2004, Pages 180-191

  Wilson, James ^a   Cuadros, Javier ^b   Cressey, Gordon ^b  

^a UNIVERSITY OF BRISTOL   (United Kingdom)

^b DEPARTMENT OF LIFE SCIENCES   (United Kingdom)

Author keywords

Dehydration; Position sensitive detector; Smectite; X ray diffraction

Indexed keywords

COMPUTATIONAL GEOMETRY; COMPUTER PROGRAMMING; COMPUTER SIMULATION; DATA ACQUISITION; DEHYDRATION; DEPOSITION; IONIZATION; PARTICLE SIZE ANALYSIS; REACTION KINETICS; X RAY DIFFRACTION;

INTERLAYER REORGANIZATIONS; INTERPARTICLE ARRANGEMENTS; POSITION SENSITIVE DETECTOR (PSD); WATER SUSPENSIONS;

CRYSTALLINE MATERIALS;

CLAY MINERAL; DEHYDRATION; MONTMORILLONITE; SMECTITE; X-RAY DIFFRACTION;

EID: 2042433661     PISSN: 00098604     EISSN: None     Source Type: Journal    
DOI: 10.1346/CCMN.2004.0520204     Document Type: Article

References (26)

1. Batchelder, M. and Cressey, G. (1998) Rapid, accurate phase quantification of clay-bearing samples using a position-sensitive X-ray detector. Clays and Clay Minerals, 46, 183-194.
2. Bergaya, F. and Vayer, M. (1997) CEC of clays: measurement by adsorption of a copper ethylenediamine complex. Applied Clay Science, 12, 275-280.
3. Blanton, T.N., Huang T.C., Toraya, H., Hubbard, C.R., Robie, S.B., Louër, D., Göbel, H.E., Will, G., Gilles, R. and Raferty, T. (1995) JCPDS - International Centre for Diffraction Data round robin study of silver behenate. A possible low-angle X-ray diffraction calibration standard. Powder Diffraction, 10, 91-95.
4. Boek, E.S., Coveney, P.V. and Skipper, N.T. (1995a) Monte Carlo molecular modeling studies of hydrated Li-, Na-, and K-smectites: Understanding the role of potassium as a clay swelling inhibitor. Journal of the American Chemical Society, 117, 12608-12617.
5. Boek, E.S., Coveney, P.V. and Skipper, N.T. (1995b) Molecular modeling of clay hydration: A study of hysteresis loops in the swelling curves of sodium montmorillonites. Langmuir, 11, 4629-4631.
6. Bradley, W.F., Grim, R.E. and Clark, G.L. (1937) A study of the behaviour of montmorillonite upon wetting. Zeitschrift Kristallographie, A97, 216-222.
7. Brindley, G.W. (1980) Quantitative X-ray mineral analysis of clays, Pp. 411-438 in: Crystal Structures of Clay Minerals and their X-ray Identification (G.W. Brindley and G. Brown, editors). Monograph 5, Mineralogical Society, London.
8. Cases, J., Bérend, I., Besson, G., François, M., Uriot, J.P., Thomas, F. and Poirier, J.E. (1992) Mechanism of adsorption and desorption of water vapor by homionic montmorillonite. 1. The sodium-exchanged form. Langmuir, 8, 2730-2739.
9. Chang, F-R.C., Skipper, N.T. and Sposito, G. (1995) Computer simulation of interlayer molecular structure in sodium montmorillonite hydrates. Langmuir, 11, 2734-2741.
10. Chatterjee, A., Iwasaki, T., Ebina, T. and Miyamoto A. (1999) A DTF study on clay-cation-water interaction in montmorillonite and beidellite. Computational Materials Science, 14, 119-124.
11. Collins, D.R., Fitch, A.N. and Catlow, R.A. (1992) Dehydration of vermiculites and montmorillonites: A time-resolved powder neutron diffraction study. Journal of Materials Chemistry, 2, 865-873.
12. da Silva, G., Fossum, J., DiMasi, E., Måløy, K. and Lutnæss, S. (2002) Synchrotron X-ray scattering studies of water intercalation in a layered synthetic silicate. Physical Review E, 66, 011303-1-011303-8.
13. DiMasi, E., Fossum, J., Gog, T. and Venkataraman, C. (2001) Orientational order in gravity dispersed clay colloids: A synchrotron X-ray scattering study of Na fluorohectorite suspension. Physical Review E, 64, 061704-1-061704-7.
14. Glaeser, R. and Méring, J. (1968) Homogeneous hydration domains of the smectites. Comptes Rendus de Seances de l'academie des sciences, Paris, 267, 436-466.
15. Howard, S.A. and Preston, K.D. (1989) Profile fitting of powder diffraction patterns. Pp. 217-276 in: Modern powder diffraction (D.L. Bish and J.E. Post, editors). Reviews in Mineralogy, 20. Mineralogical Society of America, Washington, D.C.
16. Karaborni, S., Smit, B., Heidug, W., Urai, J. and van Oort, E. (1996) The swelling of clays: molecular simulations of the hydration of montmorillonite. Science, 271, 1102-1104.
17. Kawamura, K., Ichikawa, Y., Nakano, M., Kitiyama, K. and Kawamura, H. (1999) Swelling properties of smectite up to 90°C. In-situ X-ray diffraction experiments and molecular dynamic simulations. Engineering Geology, 54, 75-79.
18. Keren, R. and Shainberg, I. (1975) Water vapor isotherms and heat of immersion of Na/Ca montmorillonite systems - I: homoionic clay. Clays and Clay Minerals, 23, 193-200.
19. MacEwan, D.M.C. and Wilson, M.J. (1980) Interlayer and intercalation complexes of clay minerals, Pp. 197-248 in: Crystal Structures of Clay Minerals and their X-ray Identification (G.W. Brindley and G. Brown, editors). Monograph 5, Mineralogical Society, London.
20. Moore, D.M. and Hower, J. (1986) Ordered interstratification of dehydrated and hydrated smectite. Clays and Clay Minerals, 34, 379-384.
21. Moore, D.M. and Reynolds, R.C. (1997) X-ray Diffraction and the Identification and Analysis of Clay Minerals. Oxford University Press, Oxford, UK.
22. Reynolds, R.C., Jr. and Reynolds, R.C., III (1996) NEWMOD: The Calculation of One-Dimensional X-ray Diffraction Patterns of Mixed-Layered Clay Minerals. Computer Program. 8 Brook Road, Hanover, New Hampshire, USA.
23. Skipper, N.T., Refson, K. and McConnell, J.D.C. (1991) Computer simulation of interlayer water in 2:1 clays. Journal of Chemical Physics, 94, 7434-7445.
24. Skipper, N., Chang, F.-R. and Sposito, G. (1995) Monte Carlo simulation of interlayer molecule structure in swelling clay minerals. 1. Methodology. Clays and Clay Minerals, 43, 285-293.
25. Sposito, G., Park, S.-H. and Sutton, R. (1999) Monte Carlo Simulation of the total radial distribution function for interlayer water in sodium and potassium montmorillonites. Clays and Clay Minerals, 47, 192-200.
26. Yamada, H., Nakazawa, H., Hashizume, H., Shimomura, S. and Watanabe, T. (1994) Hydration behavior of Na-smectite crystals synthesized at high-pressure and high-temperature. Clays and Clay Minerals, 42, 77-80.