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max of 18 keV. The spectra were summed, calibrated, and background subtracted using the Daresbury Laboratory programs EXCALIB, EXBACK, and EXSPLINE. The spectra were simulated using the EXCURV98 program (Gurman, S. J.; Binsted, N.; Ross, I. J. Phys. C 1984, 17, 143).
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4 using N-phenylanthranilic acid as an indicator.
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11244285475
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note
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2 molten sample, but 1 not the quenched form, to the need for further manipulation of the molten sample at the beamline. After packing the quenched sample under Ar in a drybox, there is no requirement for any manipulation at the beamline.
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24
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