Infrared and Raman spectroscopy of naturally occurring hydrotalcites and their synthetic equivalents

CMS Workshop Lectures

Volumn 13, Issue , 2005, Pages 204-238

  Kloprogge, J Theo ^a  

^a QUEENSLAND UNIVERSITY OF TECHNOLOGY   (Australia)

Author keywords

[No Author keywords available]

Indexed keywords

INFRARED SPECTROSCOPY; RAMAN SPECTROSCOPY;

EID: 19944368766     PISSN: 1521740X     EISSN: None     Source Type: Book Series    
DOI: 10.1346/cms-wls-13.8     Document Type: Review

References (85)

1. Alzamora, L.E., Ross, J.R., Kruissink, E.C. and Reijen, L.L.v., 1981. Coprecipitated Nickel-Alumina catalysts for methanation at high temperature. Journal of the Chemical Society, Faraday Transactions I , 77, 665-681.
2. Aminoff, G. and Broomé, B., 1931. The mineral pyroaurite Konglige Svenske Vetenskapsakademische. Handlingen, 9, p 26.
3. Aramendia, M.A. et al., 1999. Comparative study of Mg/Al and Mg/Ga layered double hydroxides. Microporous and Mesoporous Materials, 29, 319-328.
4. Banwell, C.N., 1983. Fundamentals of Molecular Spectroscopy. McGraw-Hill Book Company, London, 338 pp.
5. Barriga, C., Fernández, J.M., Ulibarri, M.A., Labajos, F.M. and Rives, V., 1996a. Synthesis and characterization of new hydrotalcite-like compounds containing Ni(II) Mn(III) in the hydroxide layers and of their calcined products. Journal of Solid State Chemistry, 124, 205-213.
6. Barriga, C., Kooli, F., Rives, V. and Ulibarri, M.A., 1996b. Layered hydroxycarbonates with the hydrotalcite structure containing Zn, Al, and Fe. In: M.L. Occelli and H. Kessler (Editors), Synthesis of Porous Materials, Zeolites, Clays, and Nanostructures. Marcel Dekker Inc., New York, pp. 661-674.
7. Bish, D.L., 1980. Anion-exchange in takovite: applications to other hydroxide minerals. Bulletin de Mineralogie, 103, 170-175.
8. Bish, D.L. and Brindley, G.W., 1977. A reinvestigation of takovite, a nickel aluminum hydroxy-carbonate of the pyroaurite group. American Mineralogist, 62, 458-464.
9. Bish, D.L. and Livingstone, A., 1981. The crystal chemistry and paragenesis of honessite and hydrohonessite: the sulphate analogues of reevesite. Mineralogical Magazine, 44, 339-343.
10. Bookin, Cherkashin, V.I. and Drits, V.A., 1993. Reinterpretation of the X-Ray diffraction patterns of stichtite and reevesite. Clays and Clay Minerals, 41, 631.
11. Brindley, G.W. and Kikkawa, S., 1979. A crystal-chemical study of Mg,Al and Ni,Al hydroxy-perchlorates and hydroxy-carbonates. American Mineralogist, 64, 836-843.
12. Bruce, L.T.J. and Turny, T.W., 1989. Cobalt clays and hydrotalcites as Fischer Tropsch catalysts, Symposium on New Catalytic Materials and Techniques. American Chemical Society, Division of Petroleum Chemistry, Miami Beach, U.S.A., pp. p 502-506.
13. Busca, G., Trifirò, F. and Vaccari, A., 1990. Characterization and catalytic activity of cobalt-chromium mixed oxides. Langmuir, 6 , 1440.
14. Chatelet, L., Bottero, J.Y., Yvon, J. and Bouchelaghem, A., 1996. Competition between monovalent and divalent anions for calcined and uncalcined hydrotalcite: anion exchange and adsorption sites. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 111, 167-175.
15. Clause, O., Gazzano, M., Trifirò, F., Vaccari, A. and Zatorski, L., 1991. Preparation and thermal reactivity of nickel/chromium and nickel/ aluminum hydrotalcite-type precursors. Applied Catalysis, 73 , 217-236.
16. Clause, O., Goncalves Coelho, M., Gazzano, M., Matteuzzi, D. and Trifiro, F., 1993. Synthesis and thermal reactivity of nickel-containing anionic clays. Applied Clay Science, 8, 169-186.
17. Corma, A., Fornes, V., Martin-Aranda, R.M. and Rey, F., 1992. Determination of base properties of hydrotalcites: Condensation of benzaldehyde with ethyl acetoacetate. Journal of Catalysis, 134 , 58-65.
18. del Arco, M., Galiano, M.V.G., Rives, V., Trujillano, R. and Malet, P., 1996. Preparation and study of decavanadate-pillared hydrotalcite-like anionic clays containing cobalt and chromium. Inorganic Chemistry, 35, 6362-6372.
19. del Arco, M., Malet, P., Trujillano, R. and Rives, V., 1999. Synthesis and characterization of hydrotalcites containing Ni(II) and Fe(III) and their calcination products. Chemistry of Materials, 11, 624-633.
20. Depége, C., Bigey, L., Forano, C., Roy, A.d. and Besse, J.P., 1996. Journal of Solid State Chemistry, 126, 314.
21. Doesburg, E.B.M., Hakvoort, G., Schaper, H. and van Reijen, L.L., 1983. The morphology of coprecipitated nickel-alumina catalysts. Applied Catalysis, 7, 85-90.
22. Drits, V.A., Sokolova, T.N., Sokolova, G.V. and Cherkashin, V.I., 1987. New members of the hydrotalcite-manasseite group. Clays and Clay Minerals, 35, 401-417.
23. Dutta, P.K. and Puri, M., 1989. Anion exchange in lithium aluminate hydroxides. Journal of Physical Chemistry, 93, 376-381.
24. Ehlsissen, K.T., Delahaye-Vidal, A., Genin, P., Figlarz, M. and Willmann, P., 1993b. Preparation and characterization of turbostratic Ni/ Al layered double hydroxides for nickel hydroxide electrode applications. Journal of Materials Chemistry, 3, 883-888.
25. 2- anion exchange during washing of Ni-Al hydroxy- compounds. Bulletin de Societe Chimique de Belge, 2, 101-107.
26. Farmer, V., 1974. The Infrared Spectra of Minerals. Mineralogical Society, England.
27. Feitknecht, W., 1942. Ueber die bildung von Doppelhydroxiden zwischen zweiun dreiwertigen Metallen. Helvetica Chimica Acta, 25, 555-560.
28. Feitknecht, W. and Gerber, M., 1942. Zur Kenntnis der Doppelhydroxyde und basischen Doppelsalze III. Ueber Magnesium-Aluminium-doppelhydroxyd. Helvetica Chimica Acta, 25, 131-137.
29. 2O. Journal of Materials Chemistry, 4, 1117-1121.
30. Fernández, J.M., Ulibarri, M.A., Labajos, F. and Rives, V., 1998. The effect of iron on the crystalline phases formed upon thermal decomposition of Mg-Al-Fe hydrotalcites. Journal of Materials Chemistry, 8, 2507-2514.
31. Frondel, C., 1941. Constitution and polymorphism of the pyroaurite and sjögrenite groups. American Mineralogist, 26, 295-315.
32. Fuda, K., Suda, K. and Matsunaga, T., 1993. Oxidation of Cr(III) to Cr(VI) species during the thermal decomposition process of Zn/Cr-layered Double Hydroxide Carbonate. Chemistry Letters, 1479.
33. Gadsden, J.A., 1975. Infrared Spectra of Minerals and Related Inorganic Compounds. Butterworths, England, 75 pp.
34. Han, K.S., Guerlou-Demourgues, L. and Delmas, C., 1997. Intercalation process of metavanadate chains into a nickel-cobalt layered double hydroxide. Solid State Ionics, 98, 85-92.
35. Hansen, H.C.B., Koch, B.C. and Taylor, R.M., 1994. Synthesis and characterization of cobalt(II)-iron(III) hydroxide carbonate: a layered double hydroxide belonging to the pyroaurite group. Journal of Solid State Chemistry, 113, 46-53.
36. Hansen, H.C.B. and Taylor, R.M., 1991a. Formation of synthetic analogues of double metal-hydroxy carbonate minerals under controlled pH conditions: II. The synthesis of desaultesite. Clay Minerals, 26, 507-525.
37. - in pyroaurite-type compounds. Clay Minerals, 26, 311-327.
38. Herman, R.G., Bogdan, C.E., Kumler, P.L. and Nuszkowski, D.M., 1993. Preparation and characterization of hydroxycarbonate precursors that yield successful alcohol synthesis catalysts. Materials Chemistry and Physics, 35, 233-239.
39. Hernandez-Moreno, M.J., Ulibarri, M.A., Rendon, J.L. and Serna, C.J., 1985. IR characteristics of hydrotalcite-like compounds. Physics and Chemistry of Minerals, 12, 34-38.
40. Hickey, L., Kloprogge, J.T. and Frost, R.L., 2000. The effects of various hydrothermal treatments on Mg/Al - hydrotalcites. Journal of Materials Science, 35, 4347-4355.
41. Hickey, L.A., Kloprogge, J.T. and Frost, R.L., 2003. The effects of synthesis pH and hydrothermal treatment on the formation of zinc aluminum hydrotalcites. Journal of Material Science, in prep.
42. Jitianu, A. et al., 2000a. Thermal behavior of hydrotalcite-like compounds: study of the resulting oxidic forms. International Journal of Inorganic Materials, 2, 287-300.
43. Jitianu, M., Jitianu, A., Zaharescu, M., Crisan, D. and Marchidan, R., 2000b. IR structural evidence of hydrotalcites derived oxidic forms. Vibrational Spectroscopy, 22, 75-86.
44. Kagunya, W., Baddour-Hadjean, R., Kooli, F. and Jones, W., 1998. Vibrational modes in Layered Double Hydroxides and their calcined derivatives. Chemical Physics, 236, 225-234.
45. Kannan, S., Narayanan, A. and Swamy, C.S., 1996. Effect of composition on the physicochemical properties of nickel aluminum hydrotalcites. Journal of Materials Science, 31, 2353-2360.
46. Kannan, S. and Swamy, C.S., 1992. Synthesis and physicochemical characterization of cobalt aluminum hydrotalcite. Journal of Materials Science Letters, 11, 1585-1587.
47. Kannan, S., Velu, S., Ramkumar, V. and Swamy, C.S., 1995. Synthesis and physicochemical properties of cobalt aluminum hydrotalcites. Journal of Materials Science, 30, 1462-1468.
48. Kloprogge, J.T. and Frost, R.L., 1999a. Fourier Transform Infrared and Raman spectroscopic study of the local structure of Mg, Ni and Co - hydrotalcites. Journal of Solid State Chemistry, 146, 506-515.
49. Kloprogge, J.T. and Frost, R.L., 1999b. Infrared Emission Spectroscopic study of the dehydroxylation of synthetic Mg/Al and Mg/Zn/Al - hydrotalcites. Physical Chemistry, Chemical Physics, 1, 1641-1647.
50. Kloprogge, J.T. and Frost, R.L., 1999c. Infrared Emission Spectroscopic study of the thermal transformation of Mg, Ni, and Co hydrotalcite catalysts. Applied Catalysis A, 184, 61-71.
51. Kooli, F., Crespo, I., Barriga, C., Ulibarri, M.A. and Rives, V., 1996. Precursor dependence of the nature and structure of non-stoichiometric magnesium aluminum vanadates. Journal of Materials Chemistry, 6 , 1199-1206.
52. 4 hydrotalcite-like compounds. Journal of Materials Science, 28, 2769-2773.
53. 3 hydrotalcite-like compounds: preparation and characterization. Journal of Materials Science, 30, 4591-4597.
54. Kooli, F., Rives, V. and Ulibarra, M.A., 1995b. Preparation and study of decavanadate-pillared hydrotalcite-like anionic clays containing transition metal cations in the layers. 2. Samples containing magnesium-chromium and nickel-chromium. Inorganic Chemistry, 34 , 5122-5128.
55. 2O, ein neues Magnesium-Aluminium-Hydroxid. Tschermaks Mineralogische und Petrographische Mitteillungen, 22, 79-87.
56. Labajos, F.M. and Rives, V., 1996. Thermal evolution of chromium(III) ions in hydrotalcite-like compounds. Inorganic Chemistry, 35 , 5313-5318.
57. 3+ in the layers and of their calcination products. Inorganic Chemistry, 35, 1154-1160.
58. 2O. Spectroscopy Letters, 24, 499-508.
59. Labajos, F.M., Rives, V. and Ulibarri, M.A., 1992. Effect of hydrothermal and thermal treatments on the physicochemical properties of Mg-Al hydrotalcite-like materials. Journal of Materials Science, 27, 1546-1552.
60. Labajos, F.M., Sastre, M.D., Trujillano, R. and Rives, V., 1999. New layered double hydroxides with the hydrotalcite structure containing Ni(II) and V(III). Journal of Materials Chemistry, 9, 1033-1039.
61. Lopez, T., Bosch, P., Asomoza, M., Gomez, R. and Ramos, E., 1997. DTA-TGA and FTIR spectroscopies of sol-gel hydrotalcites: aluminum source effect on physicochemical properties. Materials Letters, 31, 311-316.
62. Manasse, E., 1915. Idrotalcite e piroaurite. Atti della Societaa Toscana di Scienze Naturali Residente in Pisa, 24, 92-105.
63. -. Clays and Clay Minerals , 23, 369-375.
64. Miyata, S. and Kumura, T., 1973. Synthesis of new hydrotalcite-like compounds and their physico-chemical properties. Chemistry Letters , 843-848.
65. 2-. Clays and Clay Minerals, 25, 14-18.
66. Moroz, T.N. and Arkhipenko, D.K., 1991. The crystal-chemical study of natural hydrotalcites. Soviet Geology and Geophysics, 32, 52-58 (Geologiya i Geofizika UDC).
67. Mulukulta, R.S. and Detellier, C., 1996. Thermally activated Mg, Fe layered double hydroxides as reductant for nitric acid. Journal of Materials Science Letters, 15, 797.
68. Mumpton, F.A.J.H.W. and Thompson, C.S., 1965. Coalingite, a new mineral from the new Idria serpentinite, Fresno and San Benito Counties, California. American Mineralogist, 50, 1893-1913.
69. Nakamoto, K., 1997. Infrared and Raman Spectra of Inorganic and Coordination Compounds. John Wiley & Sons, USA, 84 pp.
70. Nickel, E.H. and Clarke, R.M., 1976. Carrboydite, a hydrated sulfate of nickel and aluminum: a new mineral from Western Australia. American Mineralogist, 61, 366-372.
71. Nickel, E.H. and Wildman, J.E., 1981. Hydrohonessite - a new hydrated Ni-Fe hydroxysulphate mineral; its relationship to honessite, carrboydite, and minerals of the pyroaurite group. Mineralogical Magazine, 44, 333-337.
72. Rey, F., Fornes, V. and Rojo, J.M., 1992. Thermal decomposition of hydrotalcites. An infrared and nuclear magnetic resonance spectroscopic study. Journal of the Chemical Society, Faraday Transactions, 88, 2233-2238.
73. Ross, G.J. and Kodama, H., 1967. Properties of a synthetic magensium-aluminum carbonate hydroxide and its relationship to magnesium-aluminum double hydroxide, manasseite and hydrotalcite. American Mineralogist, 52, 1036-1047.
74. Ross, S.D., 1972. Inorganic Infrared and Raman Spectra. McGraw-Hill Book Company, London, 140 pp.
75. Rousselot, I., Taviot-Gueho, C. and Besse, J.P., 1999. Synthesis and characterization of mixed Ga/Al-containing layered double hydroxides: study of their basic properties through the Knoevenagel condensation of benzaldehyde and ethyl cyanoacetate, and comparison to other LDHs. International Journal of Inorganic Materials, 1, 165-174.
76. Sato, T., Fujita, H., Endo, T. and Shimada, M., 1988. Synthesis of hydrotalcite-like compounds and their physico-chemical properties. Reactivity of Solids, 5, 219-228.
77. 3-derived compounds. Journal of Solid State Chemistry, 60, 282-288.
78. Suzuki, E., Okamoto, M. and Ono, Y., 1990. Catalysis by synthetic hydrotalcite-like materials in halide exchange between alkyl halides. Journal of Molecular Catalysis, 61, 283-294.
79. Suzuki, E. and Ono, Y., 1988. Aldol condensation reaction between formaldehyde and acetone over heat-treated synthetic hydrotalcite and hydrotalcite-like compounds. Bulletin of the Chemical Society of Japan, 61, 1008-1010.
80. Titulaer, M.K., Jansen, J.B.H. and Geus, J.W., 1994. The quantity of reduced nickel in synthetic takovite: effects of preparation conditions and calcination temperature. Clays and Clay Minerals, 42, 249-258.
81. 2O. Chemistry of Materials, 3, 626-630.
82. Vaccari, A., 1998. Preparation and Catalytic properties of cationic and anionic clays. Catalysis Today, 41, 53-71.
83. Valcheva-Traykova, M.L., Davidova, N.P. and Weiss, A.H., 1993. Thermal decomposition of Mg, Al-hydrotalcite material. Journal of Materials Science, 28, 2157-2162.
84. West, A.R., 1990. Solid State Chemistry and its Applications. Wiley & Sons, New York, 310 pp.
85. 2O. Chemistry of Materials, 10, 2277-2283.