Method for the determination of perfluorooctanoic acid in air samples using liquid chromatography with mass spectrometry

Journal of Occupational and Environmental Hygiene

Volumn 2, Issue 6, 2005, Pages 307-313

  Kaiser, Mary A ^a   Larsen, Barbara S ^a   Dawson, Barbara J ^a   Kurtz, Kristine ^b   Lieckfield Jr , Robert ^b   Miller, James R ^c   Flaherty, John ^c  

^a DUPONT COMPANY   (United States)

^b BUREAU VERITAS   (United States)

^c State College   (United States)

Author keywords

Ammonium perfluorooctanoate; Analysis; Determination; Perfluorooctanoic acid; Sampling

Indexed keywords

PERFLUOROOCTANOIC ACID; POLYSTYRENE; RESIN;

AIR SAMPLING; ANALYTIC METHOD; ARTICLE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PRIORITY JOURNAL; STANDARD; STORAGE; TEMPERATURE;

AIR POLLUTANTS, OCCUPATIONAL; CHROMATOGRAPHY, LIQUID; ENVIRONMENTAL MONITORING; FLUOROCARBONS; MASS SPECTROMETRY; OCTANOIC ACIDS; REPRODUCIBILITY OF RESULTS;

EID: 19544372949     PISSN: 15459624     EISSN: None     Source Type: Journal    
DOI: 10.1080/15459620590959713     Document Type: Article

References (17)

1. Fluoropolymer Manufacturers Group, Society of the Plastics Industry, Inc. (SPI): Detecting and Quantifying Low Levels of Fluoropolymer Polymerization Aids-A Guidance Document (BZ-102). Washington, D.C.: SPI, 2003.
2. Kissa, E.: Fluorinated Surfactants and Repellents, 2nd ed., revised, New York: Marcel Decker, Inc., 1994. p. 80.
3. Hanhijarvi, H., R.H. Ophaung, and L. Singer: The sex-related difference in perfluorooctanoate excretion in rat. Proc. Soc. Exp. Biol. Med. 171:50-55 (1982).
4. Belisle, J., and D.F. Hagen: A method for the determination of perfluorooctanoic acid in blood and other biological samples. Anal. Biochem. 101:369-376 (1980).
5. Hansen, K.J., L.A. Clemen, M.E. Ellefson, and H.O. Johnson: Compound-specific quantitative characterization of organic fluorochemicals in biological matrices. Environ. Sci. Technol. 55:766-770 (2001).
6. Olsen, G.W., K.J. Hansen, L.A. Stevenson, J.M. Burris, and J.H. Mandel: Human donor liver and serum concentrations of perfluorooctane-sulfonate and other perfluorochemicals. Environ. Sci. Technol. 35:888-891 (2003).
7. Kuklenyik, Z., J.A. Reich, J.S. Tully, L.L. Needham, and A.M. Calafat: Automated solid-phase extraction and measurement of perfluorinated organic acids and amides in human serum and milk. Environ. Sci. Technol. 38:3698-3704 (2004).
8. Giesy, J.P., and K. Kannan: Global distribution of perfluorooctane surfactants in the environment. Environ. Sci. Technol. 35:1339-1342 (2001).
9. Schultz, M.M., D.F. Barofsky, and J.A. Field: Fluorinated alkyl surfactants. Environ. Eng. Science 20:487-501 (2003).
10. Fasano, W.J., G.L. Kennedy, B. Szostek, D.G. Farrar, R.J. Ward, and L. Haroun: Penetration of ammonium perfluorooctanoate through human rat and skin in vitro. Drug Chem. Toxicol. 28:79-90 (2005).
11. Kennedy, G.L. Jr., J.L. Butenoff, G.W. Olsen, et al.: The toxicology of perfluorooctanoate. Crit. Rev. Toxicol. 54:351-384 (2004).
12. Fluoropolymer Manufacturers Group, Society of the Plastics Industry, Inc. (SPI): Guide to the Safe Handling of Fluoropolymer Dispersions (BZ-101). Washington, D.C.: SPI, 2001. p. 11.
13. American Conference of Governmental Industrial Hygienists (ACGIH®): Threshold Limit Values for Chemical Substances and Physical Agents and Biological Exposure Indices. Cincinnati, Ohio: ACGIH, 2004. p. 12.
14. Martin, J.W., D.C.G. Muir, C.A. Moody et al.: Collection of airborne fluorinated organics and analysis of gas chromatography/chemical ionization mass spectrometry. Anal. Chem. 74:584-590 (2002).
15. Kaiser, M.A., B.S. Larsen, C-P.C. Kao, and R.C. Buck: Vapor pressures of perfluoro-octanoic, -nonanoic, -decanoic, undecanoic, and dodecanoic acids. J. Chem. Eng. Data. [In review 2005].
16. Martin, J.W., K. Kannan, U. Berger et al.: Advancements in perfluoroalkyl research hampered by analytical challenges. Environ. Sci. Technol. 38:248A (2004).
17. Kennedy, E.R., T.J. Fischbach, R. Song, P.M. Eller, and S. Shulman: Guidelines for Air Sampling and Analytical Method Development and Evaluation. DHHS (NIOSH) Pub. No. 95-117. Cincinnati, Ohio: National Institute for Occupational Safety and Health, 1995. pp. 1-112.