Isolation of individual hydrocarbons from the unresolved complex hydrocarbon mixture of a biodegraded crude oil using preparative capillary gas chromatography

Organic Geochemistry

Volumn 36, Issue 6, 2005, Pages 963-970

  Sutton, P A ^a   Lewis, C A ^a   Rowland, S J ^a  

^a UNIVERSITY OF PLYMOUTH   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

CAPILLARY GAS CHROMATOGRAPHY; ELECTRON IMPACT IONIZATION; HYDROCARBON FRACTIONS; UNRESOLVED COMPLEX MIXTURE (UCM);

BIODEGRADATION; CAPILLARITY; COLUMN CHROMATOGRAPHY; CRUDE PETROLEUM; EXPLORATORY GEOCHEMISTRY; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IMPACT IONIZATION; MIXTURES;

HYDROCARBONS;

CRUDE OIL; GAS CHROMATOGRAPHY; GEOCHEMISTRY; HYDROCARBON;

EID: 18844408056     PISSN: 01466380     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.orggeochem.2004.11.007     Document Type: Article

References (36)

1. M.S. Akhlaq Rapid group-type analysis of crude oils using high-performance liquid-chromatography and gas-chromatography Journal of Chromatography A 644 1993 253 258
2. K.H. Altgelt, and M.M. Boduszynski Composition and Analysis of Heavy Petroleum Fractions 1993 Marcel Dekker New York
3. C. Armanios, R. Alexander, R.I. Kagi, and I.B. Sosrowidjojo Fractionation of sedimentary higher-plant derived pentacyclic triterpanes using molecular sieves Organic Geochemistry 21 1994 531 543
4. J. Blomberg, P.J. Schoenmakers, J. Beens, and R. Tijssen Comprehensive two-dimensional gas chromatography (GC × GC) and its applicability to the characterization of complex (petrochemical) mixtures Journal of High Resolution Chromatography 20 1997 539 544
5. Booth, A.M., 2004. Biodegradation, water solubility and characterisation studies of unresolved complex mixtures (UCMs) of aromatic hydrocarbons. Ph.D. Thesis, University of Plymouth, UK
6. S. Dagan Comparison of gas chromatography-pulsed flame photometric detection-mass spectrometry, automated mass spectral deconvolution and identification system and gas chromatography-tandem mass spectrometry as tools for trace level detection and identification Journal of Chromatography A 868 2000 229 247
7. J. Dallüge, L.L.P. van Stee, X. Xu, J. Williams, J. Beens, R.J.J. Vreuls, and U.A.Th. Brinkman Unravelling the composition of very complex samples by comprehensive gas chromatography coupled to time-of-flight mass spectrometry - cigarette smoke Journal of Chromatography A 974 2002 169 184
8. C. Demir, P. Hindmarch, and R.G. Brereton Deconvolution of a three-component co-eluting peak cluster in gas chromatography-mass spectrometry Analyst 125 2000 287 292
9. P. Donkin, E.L. Smith, and S.J. Rowland Toxic effects of unresolved complex mixtures of aromatic hydrocarbons accumulated by mussels, Mytilus edulis, from contaminated field sites Environmental Science and Technology 37 2003 4825 4830
10. L. Ellis, R. Alexander, and R.I. Kagi Separation of petroleum- hydrocarbons using dealuminated mordenite molecular-sieve. 2. Alkylnaphthalenes and alkylphenanthrenes Organic Geochemistry 21 1994 849 855
11. T. Fazeelat, R. Alexander, and R.I. Kagi Extended 8,14-secohopanes in some seep oils from Pakistan Organic Geochemistry 21 1994 257 264
12. G.S. Frysinger, R.B. Gaines, L. Xu, and C.M. Reddy Resolving the unresolved complex mixture in petroleum-contaminated sediments Environmental Science and Technology 37 2003 1653 1662
13. M.A. Gough, and S.J. Rowland Characterization of unresolved complex-mixtures of hydrocarbons in petroleum Nature 344 1990 648 650
14. M.A. Gough, M.M. Rhead, and S.J. Rowland Biodegradation studies of unresolved complex mixtures of hydrocarbons: model UCM hydrocarbons and the aliphatic UCM Organic Geochemistry 18 1992 17 22
15. J.F. Hamilton, and A.C. Lewis Monoaromatic complexity in urban air and gasoline assessed using comprehensive GC and fast GC-ToF/MS Atmospheric Environment 37 2003 589 602
16. S. Killops, and M.A.H.A. Al-Juboori Characterization of the unresolved complex mixture (UCM) in the gas chromatograms of biodegraded petroleums Organic Geochemistry 15 1990 147 160
17. S.D. Killops, and J.W. Readman HPLC fractionation and GC-MS determination of aromatic-hydrocarbons from oils and sediments Organic Geochemistry 8 1985 247 257
18. A.S. Mackenzie, C.F. Hoffman, and J.R. Maxwell Molecular parameters of maturation in the Toarcian shales, Paris Basin, France-III. Changes in aromatic steroid hydrocarbons Geochimica et Cosmochimica Acta 45 1981 1345 1355
19. K.E. Peters, and J.M. Moldowan The Biomarker Guide 1993 Prentice-Hall Englewood Cliffs, NJ pp. 245-249
20. J.B. Phillips, and J. Beens Comprehensive two-dimensional gas chromatography: a hyphenated method with strong coupling between the two dimensions Journal of Chromatography A 856 1999 331 347
21. W.G. Pool, J.W. de Leeuw, and B. van de Graaf Automated extraction of pure mass spectra from gas chromatographic mass spectrometric data Journal of Mass Spectrometry 32 1997 438 443
22. C.M. Reddy, T.I. Eglinton, A. Hounshell, H.K. White, L. Xu, R.B. Gaines, and G.S. Frysinger The West Falmouth oil spill after thirty years: the persistence of petroleum hydrocarbons in marsh sediments Environmental Science and Technology 36 2002 4754 4760
23. A.G. Requejo Quantitative analysis of triterpane and sterane biomarkers: methodology and applications in molecular maturity studies J.M. Moldowan P. Albrecht R.P. Philp Biological Markers in Sediments and Petroleum 1992 Prentice-Hall Englewood Cliffs, NJ 222 240
24. Revill, A.T., 1992. Characterisation of unresolved complex mixtures of hydrocarbons by degradative methods. Ph.D. Thesis, University of Plymouth, UK
25. S.J. Rowland, and A.T. Revill Uses of chromatography in the study of the origins and geochemistry of crude oils E. Adlard Chromatography in the Petroleum Industry. Journal of Chromatography Library Series 56 1995 Elsevier Amsterdam 127 141
26. S.J. Rowland, K. Aareskjold, G. Xuemin, and A.G. Douglas Hydrous pyrolysis of sediments - composition and proportions of aromatic-hydrocarbons in pyrolysates Organic Geochemistry 10 1986 1033 1040
27. S. Rowland, P. Donkin, E. Smith, and E. Wraige Aromatic hydrocarbon "humps" in the marine environment: unrecognized toxins? Environmental Science and Technology 35 2001 2640 2644
28. E. Smith, E. Wraige, P. Donkin, and S. Rowland Hydrocarbon humps in the marine environment: synthesis, toxicity, and aqueous solubility of monoaromatic compounds Environmental Toxicology and Chemistry 20 2001 2428 2432
29. Thomas, K.V., 1995. Characterisation and environmental effects of unresolved complex mixtures of hydrocarbons. Ph.D. Thesis, University of Plymouth, UK
30. L. Tökés, and C. Djerassi Mass spectrometry in structural and stereochemical problems. CLXXVI. Course of the electron impact induced fragmentation of androstane Journal of the American Chemical Society 91 1969 5017 5023
31. M. van Deursen, J. Beens, J. Reijenga, P. Lipman, C. Cramers, and J. Blomberg Group-type identification of oil samples using comprehensive two-dimensional gas chromatography coupled to a time-of-flight mass spectrometer (GC × GC-TOF) Journal of High Resolution Chromatography 23 2000 507 510
32. J.K. Volkman, R. Alexander, R.I. Kagi, S.J. Rowland, and P.N. Sheppard Biodegradation of aromatic hydrocarbons in crude oils from the Barrow Sub-basin of Western Australia P.A. Schenck J.W. de Leeuw G.W.M. Lijmbach Advances in Organic Geochemistry 1983 1984 Pergamon Press Oxford 619 632
33. A.M.K. Wardroper, C.F. Hoffmann, J.R. Maxwell, A.J.G. Barwise, N.S. Goodwin, and P.J.D. Park Crude oil biodegradation under simulated and natural conditions - II. Aromatic steroid hydrocarbons P.A. Schenck J.W. de Leeuw G.W.M. Lijmbach Advances in Organic Geochemistry 1983 1984 Pergamon Press Oxford 605 617
34. Warton, B., 1999. Studies of the saturate and aromatic hydrocarbon unresolved complex mixtures in petroleum. Ph.D. Thesis, Curtin University of Technology, Perth, Australia
35. B. Warton, R. Alexander, and R.I. Kagi Identification of some single branched alkanes in crude oils Organic Geochemistry 27 1997 465 476
36. B. Warton, R. Alexander, and R.I. Kagi Characterisation of the ruthenium tetroxide oxidation products from the aromatic unresolved complex mixture of a biodegraded crude oil Organic Geochemistry 30 1999 1255 1272