Use of methyl malondialdehyde as an internal standard for malondialdehyde detection: Validation by isotope-dilution gas chromatography-mass spectrometry

Clinical Chemistry

Volumn 48, Issue 12, 2002, Pages 2266-2269

  Cighetti, Giuliana ^a   Allevi, Pietro ^b   Anastasia, Luigi ^c   Bortone, Luana ^a   Paroni, Rita ^d  

^a UNIVERSITY OF MILAN   (Italy)

^b UNIVERSITY OF MILAN   (Italy)

^c PURDUE UNIVERSITY   (United States)

^d SAN RAFFAELE HOSPITAL   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

BIOLOGICAL MARKER; MALONALDEHYDE; METHYLMALONDIALDEHYDE; PHENYLHYDRAZINE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; BLOOD LEVEL; CALIBRATION; DIAGNOSTIC ACCURACY; DIAGNOSTIC VALUE; GAS CHROMATOGRAPHY; HUMAN; ISOTOPE DILUTION ASSAY; LIPID PEROXIDATION; MASS SPECTROMETRY; OXIDATIVE STRESS; QUANTITATIVE ANALYSIS; RELIABILITY; STANDARD; VALIDATION PROCESS;

EID: 18744401607     PISSN: 00099147     EISSN: None     Source Type: Journal    
DOI: 10.1093/clinchem/48.12.2266     Document Type: Article

References (15)

1. Esterbauer H, Schaur RJ, Zoller H. Chemistry and biochemistry of 4-hydroxynonenal, malondialdehyde and related aldehydes. Free Radic Biol Med 1991;11:81-128.
2. Halliwell B. Lipid peroxidation, antioxidants and cardiovascular disease: How should we move forward? Cardiovasc Res 2000;47:410-8.
3. Draper HH, Hadley M. Malondialdehyde determination as index of lipid peroxidation. Methods Enzymol 1990;186:421-31.
4. Halliwell B, Chirico S. Lipid peroxidation: Its mechanism, measurement, and significance. Am J Clin Nutr 1993;57(5 Suppl):715S-25S.
5. Pilz J, Meineke I, Gleiter CH. Measurement of free and bound malondialdehyde in plasma by high-performance liquid chromatography as the 2, 4-dinitrophenylhydrazine derivative. J Chromatogr B Biomed Sci Appl 2000; 742:315-25.
6. Cighetti G, Debiasi S, Paroni R, Allevi P. Free and total malondialdehyde assessment in biological matrices by gas chromatography-mass spectrometry: What is needed for an accurate detection. Anal Biochem 1999;266: 222-9.
7. Cavalca V, Cighetti G, Bamonti F, Loaldi A, Bortone L, Novembrino C, et al. Oxidative stress and homocysteine in coronary artery disease. Clin Chem 2001;47:887-92.
8. Cortelezzi A, Fracchiolla NS, Bamonti-Catena F, Motta M, Cighetti G, Carrabba M. et al. Hyperhomocysteinemia in myelodysplastic syndromes: Specific association with autoimmunity and cardiovascular disease. Leukemia Lymphoma 2001;41:147-50.
9. Cighetti G, Duca L, Bortone L, Sala S, Nava I, Fiorelli G, et al. Oxidative status and malondialdehyde in β-thalassaemia patients. Eur J Clin Invest 2002;32:55-60.
10. 2]-2-propenal). J Labeled Compd Radiopharm 1994;34:557-63.
11. Bull AW, Marnett LJ. Determination of malondialdehyde by ion-pairing high performance liquid chromatography. Anal Biochem 1985;149:284-90.
12. Claeson K, Thorsen G, Karlberg B. Methyl malondialdehyde as internal standard for the determination of malondialdehyde. J Chromatogr B Biomed Sci Appl 2001;751:315-23.
13. Paroni R, Fermo I, Cighetti G. Validation of methyl malondialdehyde as internal standard for malondialdehyde detection by capillary electrophoresis. Anal Biochem 2002;307:92-8.
14. Nair V, Vietti DE, Cooper CS. Degenerative chemistry of malondialdehyde. Structure, stereochemistry and kinetics of formation of enaminals from reaction with amino acids. J Am Chem Soc 1981;103:3030-6.
15. Cighetti G, Debiasi S, Ciuffreda P, Allevi P. β-ethoxyacrolein contamination increases malondialdehyde inhibition of milk xanthine oxidase activity. Free Radio Biol Med 1998;25:819-25.