Reaction of ferrocenecarboxylic acid with N,N′-disubstituted carbodiimides: Synthesis, spectroscopic and X-ray crystallographic analysis of N,N′-disubstituted N-ferrocenoylureas and identification of a one-pot coupling reagent for the formation of ferrocenecarboxamides in a non-aqueous solvent

Journal of Organometallic Chemistry

Volumn 689, Issue 9, 2004, Pages 1472-1480

  Schetter, Bernd ^a   Speiser, Bernd ^a  

^a UNIVERSITY OF TÜBINGEN   (Germany)

Author keywords

Activation; Condensation; Coupling reaction; Ferrocene; Ferrocenecarboxamide; Urea

Indexed keywords

CARBOXYLIC ACID DERIVATIVE; CYANAMIDE; DICYCLOHEXYLCARBODIIMIDE; FERROCENE DERIVATIVE; UREA DERIVATIVE;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL REACTION; CONTROLLED STUDY; CRYSTAL STRUCTURE; INFRARED SPECTROSCOPY; MASS SPECTROMETRY; PROTON NUCLEAR MAGNETIC RESONANCE; STRUCTURE ANALYSIS; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 1842716717     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jorganchem.2003.12.045     Document Type: Article

References (19)

1. Nuhn P. Naturstoffchemie 1997 157-158 S. Hirtzel Stuttgart
2. Lau H.H. Hart H. J. Org. Chem. 24 1959 280-281
3. Acton E.M. Silverstein R.M. J. Org. Chem. 24 1959 1487-1490
4. Neto A.F. Miller J. de Andrade V.F. Fujimoto S.Y. de Freitas Alfonso M.M. Archanjo F.C. Darin V.A. Andrade e Silva M.L. Borges A.D.L. Del Ponte G. Z. Anorg. Allg. Chem. 628 2002 209-216
5. Wang Q.M. Huang R.Q. J. Chem. Res. (S) 2001 246-247
6. Cooke G. Radhi A. Boden N. Bushby R.J. Lu Z. Brown S. Heath S.L. Tetrahedron 56 2000 3385-3390
7. Astruc D. Pure Appl. Chem. 75 2003 461-481
8. Pradines B. Fusai T. Daries W. Laloge V. Rogier C. Millet P. Panconi E. Kombila M. Parzy D. J. Antimicrob. Chemoth. 48 2001 179-184
9. Kovjazin R. Eldar T. Patya M. Vanichkin A. Lander H.M. Novogrodsky A. FASEB J. 17 2003 467-469
10. Mandal H.S. Kraatz H.-B. J. Organomet. Chem. 674 2003 32-37
11. Mandelbaum A. Cais M. Tetrahedron Lett. 1964 3847-3852
12. Rapić V. Filipović-Marinić N. Org. Mass Spectrom. 20 1985 104-109
13. Tenforde T. Fawwaz R.A. Freeman N.K. Castagnoli N. Jr. J. Org. Chem. 37 1972 3372-3374
14. Yavari I. Roberts J.D. Org. Chem. 43 1978 4689-4693
15. Albert, K. Fischer, G. Novak, F. Schetter, B. Speiser, B. unpublished results
16. Kupchik E.J. Kiesel R.J. J. Org. Chem. 31 1966 456-461
17. Cox R.L. Schneider T.W. Koppang M.D. Anal. Chim. Acta 262 1992 145-159
18. Oberhoff M. Duda L. Karl J. Mohr R. Erker G. Frohlich R. Grehl M. Organometallics 15 1996 4005-4011
19. Sheldrick G.M. Structure Determination and Refinement with the Program System shelx-97 1997 Universität Göttingen