Low temperature solid-state NMR experiments of half-integer quadrupolar nuclides: Caveats and data analysis

Journal of Magnetic Resonance

Volumn 168, Issue 1, 2004, Pages 66-74

  Lipton, Andrew S ^a   Heck, Robert W ^a   Sears, Jesse A ^a   Ellis, Paul D ^a  

^a PACIFIC NORTHWEST NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CAPACITORS; DATA REDUCTION; DIODES; LOW TEMPERATURE PHENOMENA; MAGNETIC FIELDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; OXIDATION; PROTEINS;

HALF-INTEGER QUADRUPOLAR NUCLIDES; PROTON CHANNEL;

ISOTOPES;

EID: 1842682333     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jmr.2004.01.008     Document Type: Article

References (26)

1. Lipton A.S., Sears J.A., Ellis P.D. A general strategy for the NMR observation of half-integer quadrupolar nuclei in dilute environments. J. Magn. Reson. 151:2001;48-59.
2. 67Zn solid-state NMR spectroscopy of the minimal DNA binding domain of human nucleotide excision repair protein XPA. J. Am. Chem. Soc. 123:2001;992-993.
3. Note that some commercially available rotary feed-thru's have magnetic components and will not hold vacuum after being inside a magnetic field.
4. Hartmann S.R., Hahn E.L. Nuclear double resonance in the rotating frame. Phys. Rev. 128:1962;2042.
5. Bak M., Rasmussen J.T., Nielsen N.C. SIMPSON: a general simulation program for solid-state NMR spectroscopy. J. Magn. Reson. 147:2000;296.
6. Pines A., Gibby M.G., Waugh J.S. Proton enhanced nuclear induction spectroscopy. A method for high resolution NMR of dilute spins in the solids. J. Chem. Phys. 56:1972;1776.
7. (a) Carr H.Y., Purcell E.M. Phys. Rev. 94:1954;630;
8. (b) Meiboom S., Gill D. Rev. Sci. Instrum. 29:1958;688.
9. 67Zn NMR spectroscopy in bioinorganic chemistry. Spectra of 4- and 6-coordinate zinc pyrazolylborate complexes obtained by management of proton relaxation rates with a paramagnetic dopant. J. Am. Chem. Soc. 124:2002;5850-5860;
10. (b) Medek A., Frydman L., Frydman l. Central transition nuclear magnetic resonance in the presences of large couplings: cobalt-59 nuclear magnetic resonance of cobaltophthalocyanines. J. Phys. Chem. 103:1999;4830-4835.
11. Larsen F.H., Jakobsen H.J., Ellis P.D., Nielsen N.C. High-field QCPMG-MAS NMR of half-integer quadrupolar nuclei with large quadrupole couplings. Mol. Phys. 95:1998;1185-1195.
12. (a) Kroeker S., Wasylishen R.E. A multinuclear magnetic resonance study of crystalline tripotassium tetracyano-cuprate. Can. J. Chem. 77:1999;1962-1972;
13. (b) Bodart P.R., Amoureux J.-P., Dumazy Y., Lefort R. Theoretical and experimental study of quadrupolar echoes for half-integer spins in static solid-state NMR. Mol. Phys. 98:2000;1545-1551
14. (c) A.S. Lipton, J.V. Hanna, in preparation.
15. (a) Cheng J.T., Edwards J.C., Ellis P.D. Measurement of quadrupolar coupling constants, shielding tensor elements and the relative orientation of quadrupolar and shielding tensor principal axis system for Rb-87 and Rb-85 nuclei in rubidium salts by solid-state NMR. J. Phys. Chem. 94:1990;553-561;
16. (b) Koons J.M., Hughes E., Cho H.M., Ellis P.D. Extracting multitensor solid-state NMR parameters from lineshapes. J. Magn. Reson. A. 114:1995;12-23;
17. 4. J. Magn. Reson. A. 122:1996;111-119.
18. (a) Vega S. Phys. Rev. 23:1981;3152;
19. (b Walter T.H., Turner G.L., Oldfield E. Oxygen-17 cross-polarization NMR spectroscopy of inorganic solids. J. Magn. Reson. 76:1988;106;
20. (c) Harris R.K., Nesbitt G.J. Cross Polarization for quadrupolar nuclei-proton to sodium-23. J. Magn. Reson. 78:1988;245-256
21. (d) Vega A. CP/MAS of quadrupolar. S=3/2 nuclei Solid State NMR. 1:1992;17.
22. (a) Ashbrook S.E., Wimperis S. Single- and multiple-quantum cross polarization in NMR of quadrupolar nuclei in static samples. Mol. Phys. 98:2000;1-26;
23. (b) Amoureux J.-P., Pruski M. Theoretical and experimental assessment of single- and multiple-quantum cross-polarization in solid state NMR. Mol. Phys. 100:2002;1595-1613.
24. J.A. Stringer, C.E. Bronnimann, Advances in RF field overlap and homogeneity in triple resonant CPMAS probes, in: Oral Presentation at the 43rd Experimental Nuclear Magnetic Resonance Conference, April 14-19, 2002.
25. A.S. Lipton, R.W. Heck, P.D. Ellis, Zinc solid-state NMR spectroscopy of human carbonic anhydrase. Implications for the enzymatic mechanism, J. Am. Chem. Soc., in press.
26. Buchko G.W., Hess N.J., Kennedy M.A. Carcinogenesis. 21:2000;1051-1057.