Homoleptic platinum(II) and palladium(II) complexes of 1,5,9- trithiacyclododecane: The crystal structures of [Pt(12S3)2](PF 6)2·2CH3NO2 and [Pd(12S3)2](BF4)2·0.5H2O

Inorganica Chimica Acta

Volumn 357, Issue 7, 2004, Pages 2107-2114

  Grant, Gregory J ^a   Goforth, Andrea M ^a   VanDerveer, Donald G ^b,c   Pennington, William T ^c  

^a UNIVERSITY OF TENNESSEE AT CHATTANOOGA   (United States)

^b GEORGIA INSTITUTE OF TECHNOLOGY   (United States)

^c CLEMSON UNIVERSITY   (United States)

Author keywords

195Pt NMR; Fluxional behavior; Palladium complexes; Platinum complexes; Thiacrowns

Indexed keywords

CHARGE TRANSFER; CHEMICAL SHIFT; CRYSTALS; ELECTROCHEMISTRY; LIGANDS; METAL COMPLEXES; METAL IONS; PLATINUM COMPOUNDS; PLATINUM METALS; SULFUR; SYNTHESIS (CHEMICAL);

ELECTRONIC SPECTROSCOPY; ELECTRONIC SPECTRUM; FLUXIONAL BEHAVIOR; NMR CHEMICAL SHIFTS; OXIDATIVE ELECTROCHEMISTRIES; PALLADIUM COMPLEXES; PLATINUM COMPLEXES; THIACROWNS;

PALLADIUM COMPOUNDS;

1,5,9 TRITHIACYCLODODECANE; CROWN ETHER DERIVATIVE; DODECANE; LIGAND; MACROCYCLIC COMPOUND; METAL COMPLEX; PALLADIUM; PALLADIUM COMPLEX; PLATINUM; PLATINUM COMPLEX; SULFIDE; SULFUR; UNCLASSIFIED DRUG; WATER;

ARTICLE; COMPLEX FORMATION; CONFORMATION; CORRELATION ANALYSIS; CRYSTAL STRUCTURE; ELECTROCHEMISTRY; ELECTRON; ENERGY TRANSFER; MOLECULAR INTERACTION; NUCLEAR MAGNETIC RESONANCE; OXIDATION; SPECTROSCOPY; SYNTHESIS;

EID: 1842636533     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ica.2003.10.033     Document Type: Article

References (40)

1. Blake A.J., Schröder M. Sykes A.G. Advances in Inorganic Chemistry. vol. 35:1990;2 Academic Press, New York.
2. Cooper S.R., Rawle S.C. Struct. Bond. (Berl.). 72:1990;1.
3. Schröder M. Pure Appl. Chem. 60:1988;517.
4. Blake A.J., Gould R.O., Holder A.J., Hyde T.I., Lavery A.J., Odulate M.O., Schröder M. J. Chem. Soc., Chem. Commun. 1987;118.
5. Blake A.J., Holder A.J., Hyde T.I., Roberts Y.V., Lavery A.J., Schröder M. J. Organometal. Chem. 323:1987;261.
6. Wieghardt K., Küppers H.-J., Raabe E., Krüger C. Angew. Chem., Int. Ed. 25:1986;1101.
7. Blake A.J., Holder A.J., Hyde T.I., Schröder M. J. Chem. Soc., Chem. Commun. 1987;987.
8. Grant G.J., Spangler N.S., Setzer W.N., VanDerveer D.G. Inorg. Chim. Acta. 246:1996;41.
9. Setzer W.N., Cacioppo E.L., Guo Q., Grant G.J., Kim D.D., Hubbard J.L., VanDerveer D.G. Inorg. Chem. 29:1990;2672.
10. Hambley T.W. Inorg. Chem. 37:1998;3767.
11. Blake A.J., Crofts R.D., Schröder M. J. Chem. Soc., Dalton Trans. 1993;2259.
12. Grant G.J., Sanders K.A., Setzer W.N., VanDerveer D.G. Inorg. Chem. 30:1991;4053.
13. Chandrasekhar S., McAuley A. Inorg. Chem. 31:1992;2663.
14. Grant G.J., Galas D.F., Jones M.W., Loveday K.D., Pennington W.T., Schimek G.L., Eagle C.T., VanDerveer D.G. Inorg. Chem. 37:1998;5299.
15. Glass R.S., Wilson G.S., Setzer W.N. J. Am. Chem. Soc. 102:1980;5068.
16. Rawle S.C., Admans G., Cooper S.R. J. Chem. Soc., Dalton Trans. 1988;93.
17. Lockhart J.C., Tomkinson N.P. J. Chem. Soc., Perkin Trans. 2:1992;533.
18. Cooper S.R., Rawle S.C., Yagbasan R., Watkin D.J. J. Am. Chem. Soc. 113:1991;1600.
19. Rawle S.C., Sewell T.J., Cooper S.R. Inorg. Chem. 26:1987;3769.
20. Cooper S.R., Rawle S.C., Hartman J.R., Hintsa E.J., Admans G.A. Inorg. Chem. 27:1988;1209.
21. Adams R.D., Layland R., McBride K. Organometallics. 15:1996;5425.
22. Adams R.D., Perrin J.L. Inorganic Syntheses. vol. 33:2002;John Wiley and Sons, New York. p. 119.
23. Pregosin P.S. Pregosin P.S. Transition Metal Nuclear Magnetic Resonance. 1991;251 Elsevier, New York. and references cited therein.
24. Sheldrick G.M. Acta Cryst. A. 46:1990;467.
25. Jacobson R.A. REQABA: Empirical Absorption Correction Version 1.1. 1998;Rigaku/Molecular Structure Corporation, The Woodlands, TX.
26. Sheldrick G.M. SHELXTL, Version 6.10 Crystallographic Computing System. 2000;Bruker AXS, Madison, WI.
27. Wilson A.J.C. International Tables for X-ray Crystallography. vol. C:1992;Kluwer Academic Publishers, Dordrecht. Table 6.1.1.4, pp. 500-502.
28. (b) Table 4.2.6.8, pp. 219-222
29. Sheldrick G.M. SHELXL-93: Program for Crystal Refinement. 1993;Gottingen University, Gottingen, Germany.
30. Blake A.J., Roberts Y.V., Schröder M. J. Chem. Soc., Dalton Trans. 1996;1885.
31. Grant G.J., Brandow C.G., Galas D.F., Davis J.P., Pennington W.T., Zubkowski J.D., Valente E.J. Polyhedron. 20:2001;3333.
32. Grant G.J., Poullaos I.M., Galas D.F., VanDerveer D.G., Zubkowski J.D., Valente E.J. Inorg. Chem. 40:2001;564.
33. Grant G.J., Poullaos I.M., Galas D.F., Carter S.C., VanDerveer D.G. J. Chem. Soc., Dalton Trans. 2002;2973.
34. Abel E.W., Beer P.D., Moss I., Orrell K.G., Sik V., Bates P.A., Hurthouse M.B. J. Chem. Soc., Chem. Commun. 1987;978.
35. Nikol H., Bürgi H., Hardcastle K.I., Gray H.B. Inorg. Chem. 34:1995;6319.
36. Gelling A., Olsen M., Orrell K.G., Osborne A.G., Sik V. J. Chem. Soc., Chem. Commun. 1997;587.
37. Abel E.W., Gelling A., Orrell K.G., Osborne A.G., Sik V. J. Chem. Soc., Chem. Commun. 1996;2329.
38. Abel E.W., Moss I., Orrell K.G., Qureshi K.B., Sik V., Stephenson D. J. Chem. Soc., Dalton Trans. 1988;1489.
39. Carrion M.C., Jalon F.A., Manzano B.R., de la Hoz A., Claramunt R.M., Milata V., Elguero J. Inorg. Chem. 42:2003;885.
40. Blake A.J., Holder A.J., Reid G., Schröder M. J. Chem. Soc., Dalton Trans. 1994;627.