Polymorphism in dinuclear Cu(II) compounds - Polymorphism caused by different degrees of hydration: The structures of [Cu(HL)]2Cl 24H2O (I), [Cu(HL)]2Cl 2·2H2O (II), [Cu(HL)]2)(NO3)2· 4H2O (III), [Cu(HL)]2)(NO3)2·2H2O (IV) and [Cu(HL)]2)(ClO4)2· 2H2O (V)(HL=[(3-aminopropyl)-di-(2-hydroxopropyl)]amine anion). Counterion control of the crystallization pathway. Part 11

Inorganica Chimica Acta

Volumn 357, Issue 5, 2004, Pages 1360-1368

  Mukhopadhyay, Uday ^a   Bernal, Ivan ^a  

^a University of Houston   (United States)

Author keywords

Dinuclear Cu(II) complexes; Hydration polymorphism; Magnetism; X ray crystallography

Indexed keywords

CHLORINE COMPOUNDS; CHROMIUM COMPOUNDS; HYDRATION; MAGNETIC MOMENTS; MAGNETISM; NEGATIVE IONS; ORGANIC SOLVENTS; POLYMORPHISM; POSITIVE IONS; X RAY CRYSTALLOGRAPHY;

ANTIFERRO-MAGNETICALLY COUPLED; COUNTER ANIONS; CRYSTALLIZATION PATHWAY; CU COMPLEXES; DEGREES OF HYDRATION; FROZEN SOLUTIONS; METALLIC CORES; POLYMORPHIC FORMS;

COPPER COMPOUNDS;

COPPER DERIVATIVE; METHANOL; PROPYLAMINE; WATER;

ACCURACY; ARTICLE; CHEMICAL BOND; CHEMICAL COMPOSITION; CHEMICAL REACTION; CRYSTAL STRUCTURE; CRYSTALLIZATION; HYDRATION; MAGNETISM; MODEL; REACTION ANALYSIS; STEREOCHEMISTRY; STRUCTURE ANALYSIS; X RAY CRYSTALLOGRAPHY;

EID: 1842421380     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ica.2003.11.037     Document Type: Article

References (40)

1. Giacovazzo C., Monaco H.L., Viterbo D., Scordari F., Gilli G., Zanotti G., Cati M., Giacovazzo C. Fundamentals of Crystallography. 1992;482 Oxford University Press.
2. Bernal I., Clearfield A., Epstein E.F., Ricci J.S. Jr., Balch A., Miller J.S. Chem. Commun. 1973;39.
3. Clearfield A., Epstein E.F., Bernal I. J. Coord. Chem. 6:1977;227.
4. Bernal I., Somoza F., Chen Y.-C., Massoud S.S. J. Coord. Chem. 41:1997;233.
5. Nakai H., Shiro M., Ezumi K., Sakata S., Kubota T. Acta Cryst. B. 32:1976;1827.
6. Nakai H., Ezumi K., Shiro M. Acta Cryst. B. 37:1981;193.
7. Bernal I., Korp J.D., Schlemper E.O., Hussain M.S. Polyhedron. 1:1982;365.
8. Aoyama T., Ohba S., Saito T., Bernal I. Acta Crystal. C. 48:1992;246.
9. Bernal I., Yufit D.S., Howard J.A.K. Z. Kristallogr. 216:2001;413.
10. The Cambridge Structural Database, 12 Union Road, Cambridge CB2 1EZ, UK
11. Shekunov B.Y. J. Cryst. Growth. 211(1-4):2000;122.
12. Garcia E. J. Cryst. Growth. 198/199(Pt. 2):1999;1360.
13. Foreman J.et al. Drug Discov. Develop. 1998;52.
14. M.C. Wahle, 1997
15. Hanioka N.et al. Am. J. Hum. Genet. 47(6):1990;994.
16. Gough C.A.et al. Nature (London). 347(6295):1990;773.
17. Guengerich F.P.et al. Biochem. Soc. Trans. 15(4):1987;576.
18. C.A. Miller, 1984
19. Byrn R.S.et al. J. Pharm. Sci. 74(5):1985;565.
20. Larrey D.et al. Biochemistry. 23(12):1984;2787.
21. Sjoeqvist F. Biochem. Soc. Trans. 12(1):1984;101.
22. Penno M.B.et al. J. Clin. Invest. 71(6):1983;1698.
23. Sloan T.P.et al. Br. Med. J. 2(6138):1978;655.
24. Drayer D.E.et al. Clin. Pharmacol. Ther. 22(3):1977;251.
25. Affonso A.et al. J. Pharm. Sci. 60(10):1971;1572.
26. Bernstein J. Polymorphism in Molecular Crystals. 2002;Oxford University Press. ISBN 0198506058.
27. Bernal I. J. Coord. Chem. 15:1987;337.
28. Solution, refinement and graphics were carried out with the various routines available in L. Farrugia's University of Glasgow, package WINGX. See Farrugia L. J. Appl. Crystallogr. 32:1999;837.
29. Structural Solution and Refining: Sheldrick G.M. SHELXS 97, Program for the Solution of Crystals Structures and SHELXL 97: Program for the Refinement of Crystal Structures. 1997;University of Göttingen, Germany.
30. A. Altomare, M.C. Burla, M. Camalli, G. Cascarano C. Giacovazzo. A. Guagliardi, A.G.G. Moliterni, G., Polidori, R. Spagna, SIR92: A Program for Solving and Refining Crystals Structures
31. Graphics: N.B. Michael, K.J. Carroll, ORTEP-III Oak Ridge Thermal Ellipsoid Plot Program for Crystal Structure Illustrations, Oak Ridge National Laboratory Report ORNL-6895, 1996 (a printed reference manual is available). Available from http://www.ornl.gov/ortep/ortep.html
32. Spek A.L. PLATON: Multipurpose Crystallographic Tool. 1999;Utrecht University, Utrecht, The Netherlands.
33. Kahn O. Molecular Magnetism. 1993;VCH Publishers, New York. see pp. 107 and 159.
34. Ikeda K., Ohba M., Ōkawa H. J. Chem. Soc., Dalton Trans. 2001;3119.
35. Gupta R., Mukherjee S., Mukherjee R. J. Chem. Soc., Dalton Trans. 1999;4025.
36. Azari S.K.S., Roy T.G., Dey B.K., Das S.C., Tiekink E.R.T. Metal Based Drugs. 4:1997;255.
37. Petrovcic N., Kozlevcar B., Golic L., Leban I., Segedin P. Acta Crystal. C. 55:1999;176.
38. Pariya C., Liao F., Wangand S.L., Chung C.S. Polyhedron. 17:1998;547.
39. Bonamartini A.C., Bruni S., Cariati F., Battaglia L.P., Pelosi G. Inorg. Chim. Acta. 205:1993;99.
40. Walsh J., Hathaway B.J. J. Chem. Soc., Dalton Trans. 1984;15.