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27844557060
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note
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3CN used for the solutions and for synthesis was dried by CaH2 and distilled twice (the second time inside the glovebox) under argon atmosphere.
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19
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27844563286
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note
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The pyrex tubes were perfectly airtight, being closed by greased Schlenk-type threaded ground glass joints equipped with an o-ring.
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20
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22
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27844564951
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note
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Anal calc: C, 55.3; H, 6.45; N, 3.23; O, 7.4; S, 14.8; Fe, 12.9. Found: C, 55.5; H, 6.33; N, 3.48; O, 8.78; S, 15.8; Fe, 12.3.
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23
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0001391285
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Huang, L.R.6
Huang, Z.Y.7
Liu, H.Q.8
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