Structural characterization of poly(diethylsiloxane) in the crystalline, liquid crystalline and isotropic phases by solid-state 17O NMR spectroscopy and ab initio MO calculations

Magnetic Resonance in Chemistry

Volumn 43, Issue 3, 2005, Pages 209-216

  Kimura, Hideaki ^a   Kanesaka, Sho ^a   Kuroki, Shigeki ^a   Ando, Isao ^a   Asano, Atsushi ^b   Kurosu, Hiromichi ^c  

^a TOKYO INSTITUTE OF TECHNOLOGY   (Japan)

^b NATIONAL DEFENSE ACADEMY   (Japan)

^c NARA WOMEN'S UNIVERSITY   (Japan)

Author keywords

Ab initio MO calculations; PDES; Poly(diethylsiloxane); Solid state 17O NMR; Structural characterization

Indexed keywords

CATIONIC POLYMERIZATION; ELECTRIC FIELDS; LIGHT POLARIZATION; LIQUID CRYSTALS; MOLECULAR ORBITALS; RING OPENING POLYMERIZATION; TEMPERATURE;

AB INITIO MOLECULAR ORBITAL CALCULATION; ISOTROPIC PHASIS; LIQUID-CRYSTALLINE PHASIS; POLY(DI-ETHYLSILOXANE); POLY(DIETHYLSILOXANE); SOLID STATE NMR; SOLID-STATE 17O NMR; STRUCTURAL CHARACTERIZATION;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

CARBON 13; HYDROGEN; OXYGEN; OXYGEN 17; POLY(DIETHYLSILOXANE); POLYMER; SILICON DERIVATIVE; SILOXANE; UNCLASSIFIED DRUG; BAYSILON; DIMETICONE; SILICONE DERIVATIVE;

AB INITIO CALCULATION; ARTICLE; CHEMICAL STRUCTURE; DYNAMICS; ELECTRIC FIELD; HIGH TEMPERATURE; MOLECULAR WEIGHT; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYMERIZATION; PROTON NUCLEAR MAGNETIC RESONANCE; SOLID STATE; STATISTICAL SIGNIFICANCE; TEMPERATURE; CHEMISTRY; COMPUTER SIMULATION; CONFORMATION; CRYSTALLOGRAPHY; METHODOLOGY; PHASE TRANSITION; SOLUTION AND SOLUBILITY;

COMPUTER SIMULATION; CRYSTALLOGRAPHY; DIMETHYLPOLYSILOXANES; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, MOLECULAR; MOLECULAR CONFORMATION; OXYGEN; OXYGEN ISOTOPES; PHASE TRANSITION; SILICONES; SOLUTIONS;

EID: 18044370470     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/mrc.1527     Document Type: Article

References (45)

1. Brook AB. Silicon in Organic, Organometallic, and Polymer Chemistry. John Wiley: New York, 2000.
2. Teyssie D, Boileau S. In Silicon-Containing Polymer; Jones RG, Ando W, Chojnowski J (eds). Kluwer Academic: Dordrecht, 2000; 593.
3. Godovsky YK, Papkov VS. Adv. Polym. Sci. 1989; 88: 129.
4. Harkness BR, Tachikawa M, Yue H, Mita I. Chem. Mater. 1998; 10: 1700.
5. Molenberg A, Möller M. Macromolecules 1997; 30: 8332.
6. Out GJJ, Turetskii AA, Möller M. Macromol. Rapid Commun. 1995; 16: 107.
7. Out GJJ, Klok HA, Möller M. Macromol. Cem. Phys. 1995; 196: 196.
8. Out GJJ, Turetskii AA, Möller M, Oelfin D. Macromolecules 1994; 27: 3310.
9. Kögler G, Loufakis K, Möller M. Polymer 1990; 31: 1538.
10. Möller M, Siffrin S, Kögler G, Oelfin D. Macromol. Cem. Macromol. Symp. 1990; 34: 171.
11. Kögler G, Hasenhindl A, Möller M. Macromolecules 1989; 22: 4190.
12. Litvinov VM, Whittaker AK, Hagemeyer A, Spiess HW. Colloid Polym. Sci. 1989; 267: 681.
13. Friedrich J, Rabolt JF. Macromolecules 1987; 20: 1975.
14. Papkov VS, Svistunov VS, Godovsky YK, Zhdanov AA. J. Polym. Sci. (B) 1987; 25: 1859.
15. Godovsky YK, Papkov VS. Macromol. Cem. Macromol. Symp. 1986; 4: 71.
16. Tsvankin DY, Papkov VS, Zhukov VP, Godovsky YK, Svistunov VS, Zhdanov AA. J. Polym. Sci.: Polym. Chem. Ed. 1985; 23: 1043.
17. Godovsky YK, Makarova NN, Papkov VS, Kuzmin NN. Macromol. Cem. Rapid. Commun. 1985; 6: 443.
18. Papkov VS, Godovsky YK, Svistunov VS, Litvinov VM, Zhdanov AA. J. Polym. Sci.: Polym. Chem. Ed. 1984; 22: 3617.
19. Grinberg F, Kimmich R, Möller M, Molenberg A. J. Chem. Phys. 1996; 105: 9657.
20. Kimmich R, Stapf S, Möller M, Out R, Seitter R-O. Macromolecules 1994; 27: 1505.
21. Litvinov VM, Macho V, Spiess HW. Acta Polym. 1997; 48: 471.
22. Miller RD, Hofer D, Rabolt JF, Fickes GN. J. Am. Chem. Soc. 1985; 107: 2172.
23. Karikari EK, Greso AJ, Farmer BL, Miller RD. Macromolecules 1993; 26: 3937.
24. Miller RD, Michl J. Chem. Rev. 1989; 89: 1359.
25. Papkov VS, Il'ina MN, Zhukov VP, Tsvankin DJ, Tur DR. Macromolecules 1992; 25: 2033.
26. Kanesaka S, Kimura H, Kuroki S, Ando I, Fujishige S. Macromolecules 2004; 37: 453.
27. Kuroki S, Yamauchi K, Ando I, Shoji A, Ozaki T. Curr. Org. 2001; 5: 1001.
28. Yamauchi K, Kuroki S, Ando I. J. Mol. Struct. 2002; 602/603: 171.
29. Yamauchi K, Kuroki S, Ando I, Shoji A, Ozaki T. Chem. Phys. Lett. 1999; 302: 331.
30. Kuroki S, Takahashi A, Ando I, Shoji A, Ozaki T. J. Mol. Struct. 1994; 323: 197.
31. Emsley JW. In Encyclopedia of NMR, Vol. 3, Grant DM, Harris RK (eds). John Wiley: Chichester, 1996; 2788-2799.
32. Lafuma A, Fayon F, Massiot D, Kimmés SC, Sanchez C. Magn. Reson. Chem. 2003; 41: 944.
33. Clark TM, Grandinetti PJ, Florian P, Stebbins JF. J. Phys. Chem. B 2001; 105: 12 257.
34. Vermillion KE, Florian P, Grandinetti PJ. J. Chem. Phys. 1998; 108: 7274.
35. Young CW, Servais PC, Currie CC, Hunter MJ. J. Am. Chem. Soc. 1948; 70: 3758.
36. Mark JE, Chin DS, Su TK. Polymer 1978; 19: 407.
37. Godovsky YK, Papkov VS. Poly(diethylsiloxane): http://www.oup-usa.org/ pdh/PDH-725.PDF.
38. Bielecki A, Burum DP. J. Magn. Reson. 1995; A116: 215.
39. van Gorkom LCM, Hook JM, Logan MB, Hanna JV, Wasylishen RE. Magn. Reson. Chem. 1995; 33: 791.
40. van Eck ERH, Smith ME. J.Chem.Phys. 1998; 108: 5904.
41. Ashbrook SE, Wimperis S. J.Magn.Reson. 2000; 147: 238.
42. Massiot D, Fayon F, Capron M, King I, Calvé Alonso B, Durand J-O, Bujoli B, Gan Z, Hoatson G. Magn. Reson. Chem. 2002; 40: 70.
43. Wu G, Hook A, Dong S, Yamada K. J. Phys. Chem. A 2000; 104: 4102.
44. Mehring M. High Resolution NMR of Solids. Springer: Berlin, 1983; 8-62.
45. Fyfe CA. Solid State NMR for Chemists. CFC Press: Guelph, Canada, 1983.