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Volumn 13, Issue 10, 2005, Pages 3467-3473

An efficient preparation of polyanionic affinity agent and its evaluation for the measurement of glycated hemoglobin

Author keywords

Diabetes mellitus; Glycated hemoglobin; Polyanionic affinity agent

Indexed keywords

BORONIC ACID DERIVATIVE; GLYCOSYLATED HEMOGLOBIN; POLYANION;

EID: 17444410306     PISSN: 09680896     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.bmc.2005.02.058     Document Type: Article
Times cited : (3)

References (44)
  • 7
    • 85030798523 scopus 로고    scopus 로고
    • National Diabetes Information Clearinghouse. Diabetes Overview
    • National Diabetes Information Clearinghouse. Diabetes Overview at http://www.niddk.nih.gov/health/diabetes/diabetes.htm
  • 33
    • 17444403655 scopus 로고
    • For preparation of different polymeric boronic acid derivatives, see: J. Solms, and H. Deuel Chemia 11 1957 311
    • (1957) Chemia , vol.11 , pp. 311
    • Solms, J.1    Deuel, H.2
  • 43
    • 85030795898 scopus 로고    scopus 로고
    • note
    • The theoretical yield of powdered polymeric affinity agent (3) was calculated based on a reaction between acrylic acid monomer (MW: 72.06) and 3-aminophenylboronic acid hemisulfate (2, MW: 186.0) with the loss of water
  • 44
    • 85030799053 scopus 로고    scopus 로고
    • note
    • -1 was used for calculation. The extinction coefficient (ε) was determined based on two model conjugates, 3-(dihydroxyboryl)acetamide (derivative of acetic acid) and 5-{[3-(dihydroxy boryl)phenyl]amino}-5-oxo-3-phenylpentanoic acid (derivative of glutaric acid) in taurine buffer (50 mM, pH 9.0) at 252 nm. The elemental analysis method for determination of boronic acid incorporation ratio was based on observed values versus the theoretical values of a statistical mixture of acrylic acid and its 3-aminophenylboronic acid derivative, 3-(dihydroxyboryl) acrylamide


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.