HPLC-based procedure for the preparation of carbene-generating photoreactive GM3 and GM1 ganglioside derivatives radioiodinated to high specific radioactivity with chloramine T as an oxidant

Analytical Biochemistry

Volumn 340, Issue 2, 2005, Pages 373-375

  Panasiewicz, Miroslawa ^a   Mieczkowski, Józef ^b   Domek, Hanna ^a   Pacuszka, Tadeusz ^a  

^a MEDICAL CENTER FOR POSTGRADUATE EDUCATION   (Poland)

^b UNIVERSITY OF WARSAW   (Poland)

Author keywords

[No Author keywords available]

Indexed keywords

BIOCHEMISTRY;

CARBENES; CHLORAMINE-T; SPECIFIC RADIOACTIVITY;

CHEMISTRY;

CARBENE; FATTY ACID DERIVATIVE; GANGLIOSIDE; GANGLIOSIDE GM1; GANGLIOSIDE GM3; OXIDIZING AGENT; TOSYLCHLORAMIDE SODIUM;

ACCURACY; ACYLATION; ANIMAL CELL; ARTICLE; CALCULATION; CHEMICAL ANALYSIS; CHEMICAL PROCEDURES; CHROMATOGRAPHY; CONTROLLED STUDY; ELECTROSPRAY MASS SPECTROMETRY; ELUTION; ERYTHROCYTE; GEL PERMEATION CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IODINATION; MATERIALS; MOLECULE; NONHUMAN; PH; PHOTOREACTIVITY; PRIORITY JOURNAL; PURIFICATION; RADIOACTIVITY; RADIOIODINATION; ROOM TEMPERATURE; SAFETY; STANDARD; TECHNIQUE;

ANIMALIA;

EID: 17444395238     PISSN: 00032697     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ab.2004.11.044     Document Type: Article

References (9)

1. M.M.P. Zegers, J.W. Kok, and D. Hoekstra Use of photoactivable sphingolipid analogues to monitor lipid transport in mammalian cells Biochem. J. 328 1997 489 498
2. P. Palestini, M. Pitto, G. Tedeschi, A. Ferraretto, M. Parenti, J. Brunner, and M. Masserini Tubulin anchoring to glycolipid-enriched, detergent-resistant domains of the neuronal plasma membrane J. Biol. Chem. 275 2000 9978 9985
3. M. Wendeler, J. Hoerschemeyer, D. Hoffmann, T. Kolter, G. Schwarzmann, and K. Sandhoff Photoaffinity labelling of the human GM2-activator protein: mechanistic insight into ganglioside GM2 degradation Eur. J. Biochem. 271 2004 614 627
4. T. Weber, and J. Brunner 2-(Tributylstannyl)-4-[3-(trifluoromethyl)-3H- diazirin-3-yl]benzyl alcohol: a building block for photolabeling and cross-linking reagents of very high specific radioactivity J. Am. Chem. Soc. 117 1995 3084 3095
5. T. Pacuszka, R.O. Duffard, R.N. Nishimura, R.O. Brady, and P.H. Fishman Biosynthesis of bovine thyroid gangliosides J. Biol. Chem. 253 1978 5839 5846
6. G. Schwarzmann, and K. Sandhoff Lysogangliosides: synthesis and use in preparing labeled gangliosides Methods Enzymol. 138 1987 319 341
7. G. Gazotti, S. Sonnino, R. Ghidoni, and G. Tettamanti Analytical and preparative high performance liquid chromatography of gangliosides J. Neurosci. Res. 12 1984 179 192
8. M. Panasiewicz, H. Domek, G. Hoser, M. Kawalec, and T. Pacuszka Structure of the ceramide moiety of GM1 ganglioside determines its occurrence in different detergent-resistant membrane domains in HL-60 cells Biochemistry 42 2003 6608 6619
9. S.M. Moerlein, W. Beyer, and G. Stöcklin No-carrier-added radiobromination and radioiodination of aromatic rings using in situ generated peracetic acid J. Chem. Soc. Perkin Trans. 1 1988 779 786