Supercritical CO2 improved phosphine imide reaction on peracetylated β-cyclodextrin

Tetrahedron Letters

Volumn 46, Issue 19, 2005, Pages 3307-3309

  Menuel, Stephane ^a   Wagner, Michel ^a   Barth, Danielle ^b   Marsura, Alain ^a  

^a NANCY UNIVERSITÉ   (France)

^b Lab Thermodyn Milieux Polyphases   (France)

Author keywords

Cyclodextrin; Phosphine imide reaction; Supercritical CO2

Indexed keywords

BETA CYCLODEXTRIN DERIVATIVE; CARBON DIOXIDE; IMIDE; PHOSPHINE DERIVATIVE; POLYMER; UREA; UREA DERIVATIVE;

ARTICLE; CHEMICAL REACTION; POLYMER PRODUCTION; REACTION ANALYSIS; SUBSTITUTION REACTION; SUPERCRITICAL FLUID; SYNTHESIS;

EID: 17344365356     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2005.03.107     Document Type: Article

References (11)

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10. 2 can enter from the top or the bottom; a sampling section, composed of different valves which allow the recovery of the products at the end of the reaction. Whole apparatus used for the reaction under pressure: (A) compression modulus; (B) reaction modulus (batch reactor = I.D. = 4 cm, height = 8 m); Sampling modulus
11. A); 34.2; 32.4, 26.0, 25.3 (cyclohexyl); 21.2-20.9 (multiple s, MeCO).