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17144423429
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note
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A THF solution (1.0 mL) of 1 (0.195 g, 0.20 mmol), a 1,3-diene (0.90 mmol), 18-Crown-6 (0.334 g 1.26 mmol) and KF (0.071 g, 1.23 mmol) was stirred for the time specified in Scheme 2. The mixture was diluted with ethyl acetate, washed with brine and concentrated. The residue was purified by GPC to give the corresponding product.
-
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17
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17144380263
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note
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54: 1062.4226, Found 1062.4240.
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