Qualitative and quantitative analysis by hyphenated (HP)TLC-FTIR technique

Journal of Liquid Chromatography and Related Technologies

Volumn 28, Issue 7-8, 2005, Pages 1203-1213

  Cimpoiu, Claudia ^a  

^a BABE BOLYAI UNIVERSITY   (Romania)

Author keywords

High performance thin layer chromatography; Hyphenated techniques; IR spectroscopy; Qualitative analysis; Quantitative analysis; Thin layer chromatography

Indexed keywords

DRUG PRODUCTS; ENVIRONMENTAL IMPACT; FOOD PRODUCTS; FOURIER TRANSFORM INFRARED SPECTROSCOPY; INFRARED SPECTROSCOPY; MOLECULAR STRUCTURE; SPECTROMETRY;

BIOLOGICAL ANALYSIS; DRUG ANALYSIS; FOOD ANALYSIS; FORENSIC ANALYSIS;

THIN LAYER CHROMATOGRAPHY;

AMPHETAMINE; BENZODIAZEPINE; HEXOBARBITAL; INDOLE DERIVATIVE; MORPHINE; PHENOBARBITAL; SALICYLIC ACID;

CHEMICAL STRUCTURE; DATA ANALYSIS; ENVIRONMENTAL FACTOR; FOOD ANALYSIS; HIGH PERFORMANCE THIN LAYER CHROMATOGRAPHY; INFRARED SPECTROSCOPY; INSTRUMENTATION; INTERFEROMETER; METHODOLOGY; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; REVIEW; THIN LAYER CHROMATOGRAPHY;

EID: 17044385416     PISSN: 10826076     EISSN: None     Source Type: Journal    
DOI: 10.1081/JLC-200053025     Document Type: Review

References (26)

1. Gocan, S.; Cimpan, G. Compound identification in thin layer chromatography using spectrometric methods. Rev. Anal. Chem. 1997, XVI, 1-24b.
2. Csehati, T.; Forgacs, E. Hyphenated techniques in thin layer chromatography. J. Assoc. Off. Anal. Chem. 1998, 81, 329-332.
3. Somsen, G.W.; Visser, T. Liquid Chromatography/Infrared Spectroscopy. In Encyclopedia of Analytical Chemistry; Meyers, R.A., Ed.; John Wiley & Sons Ltd: Chichester, 2003.
4. Somsen, G.W.; Morden, W.; Wilson, I.D. Planar chromatography coupled with spectroscopic techniques. J. Chromatogr. 1995, 703, 613-665.
5. Rager, I.O.C.; Kovar, K.-A. Planar Chromatography and IR. In Planar Chromatography; Nyiredy, Sz., Ed.; Springer Scientific Publisher: Budapest, Hungary, 2001.
6. Glauninger, G.; Kovar, K.-A.; Hoffmann, V. Untersuchungen zum online DC-IR Transfer. In Software Entwicklungen in der Chemie 3. Proceeding of 3rd Workshop Comput. Chem., Berlin, Germany; Gauglitz, G., Eds.; Springer: Berlin, 1989.
7. Pfeifer, A.; Tolimann, G.; Ammon, H.P.T.; Kovar, K.A. Identification of adenosine in biological samples by HPTLC-FTIR on-line coupling. J. Planar Chromatogr.-Mod. TLC 1996, 9, 31-34.
8. Stahlmann, S.; Kovar, K.A. Analysis of impurities by high-performance thin-layer chromatography with fourier transform infrared spectroscopy and UV absorbance detection in situ measurement: chlordiazepoxide in bulk powder and in tablets. J. Chromatogr., A 1998, 813, 145-152.
9. Bayerbach, S.; Gauglitz, G.; Kovar, K.-A.; Pisternick, W. Spektrale Detektion in der Dünnschichtchromatographie-Vergleich UV/VIS und IR. In Dünnschichtchromatographie in memoriam Professor Dr Jork; Kaiser, R.E., Günther, W., Gunz, H., Wulff, G., Eds.; InCom Sonderband, 1995.
10. Bauer, G.K.; Pfeifer, A.M.; Hauck, H.E.; Kovar, K.-A. Development of an optimized sorbent for direct HPTLC-FTIR on-line coupling. J. Planar Chromatogr.-Mod. TLC 1998, 11, 84-89.
11. Bauer, G.K.; Kovar, K.-A. Direct HPTLC-FTIR on-line coupling: interaction of acids and bases with the binder in precoated HPTLC plates. J. Planar Chromatogr.-Mod. TLC 1999, 11, 30-33.
12. Griffiths, P.R.; de Haseth, J.A. Fourier Transform Infrared Spectrometry; Wiley-Interscience: New York, USA, 1986.
13. Kovar, K.-A.; Hoffmann, V. Möglichkeiten und Grenzen der direkten DC-FTIR Kopplung. GIT Spezial Chromatographie 1991, 11, 1197-1201.
14. Morlock, G.; Kovar, K.-A. Detection, identification, and documentation. In Handbook of Thin Layer Chromatography; Sherma, J., Fried, B., Eds.; Marcel Dekker Inc.: New York, USA, 2003.
15. Kovar, K.-A.; Dinkelacker, I.; Pfeifer, A.; Pisternick, W.; Wössner, A. Identifizierung von Suchstoffen mit Hilfe der HPTLC-UV/IR-Kopplung. GIT Spezial Chromatographie 1995, 15, 19-24.
16. Kovar, K.-A.; Enßlin, H.K.; Frey, O.R.; Rienas, S.; Wolff, S.C. Die direkte DC-IR-Kopplung zur Identifizierung und Bestimmung von Substanzgemischen. GIT Spezial Chromatographie 1991, 11, 95-101.
17. Cimpoiu, C.; Miclaus, V.; Damian, G.; Puia, M.; Casoni, D.; Bele, C.; Hodisan, T. Identification of new phtalazine derivatives by HPTLC-FTIR and characterization of their separation using some molecular properties. J. Liq. Chromatogr. & Rel. Technol. 2003, 26, 2687-2696.
18. Cserhati, T.; Forgacs, E.; Candeias, M.; Vilas-Boas, L.; Bronze, R.; Spranger, I. Separation and tentative identification of the main pigment fraction of raisins by thin-layer chromatography-fourier transform infrared and high performance liquid chromatography-ultraviolet detection. J. Chromatogr. Sci. 2000, 38, 145-150.
19. Cserhati, T.; Forgacs, E.; Morais, M.H.; Ramos, A.C. TLC-FTIR of color pigments of chestnut sawdust. J. Liq. Chromatogr. & Rel. Technol. 2001, 24, 1435-1445.
20. 9- tetrahydrocannabinol-9-carboxylic acid in urine by use of HPTLC-UV/FTIR on-line coupling. J. Planar Chromatogr.-Mod. TLC 1997, 10, 348-352.
21. Pfeifer, A.M.; Kovar, K.-A. Identification of LSD, MBDB, and atropine in real samples with on-line HPTLC-FTIR coupling. J. Planar Chromatogr.-Mod. TLC 1995, 8, 388-392.
22. Pisternick, W.; Kovar, K.-A.; Ensslin, H. High-performance thin-layer chromatogeaphic determination of N-ethyl-3,4-methylenedioxy-amphetamine and its major metabolites in urine and comparison with high performance liquid chromatography. J. Chromatogr. B 1997, 688, 63-69.
23. Stahlmann, S.A. Ten-year report on HPTLC-FTIR online coupling. J. Planar Chromatogr.-Mod. TLC 1999, 12, 5-12.
24. Frey, O.R.; Kovar, K.-A.; Hoffmann, V. Possibilities and limitations of assays by on-line coupling of thin layer chromatography and FTIR spectroscopy. J. Planar Chromatogr.-Mod. TLC 1993, 6, 93-99.
25. Wolff, S.C.; Kovar, K.-A. Determination of edetic acid (EDTA) in water by on-line coupling of HPTLC and FTIR. J. Planar Chromatogr.-Mod. TLC 1994, 7, 286-290.
26. Wolff, S.C.; Kovar, K.-A. Direct HPTLC-FTIR measurement in combination with AMD. J. Planar Chromatogr.-Mod. TLC 1994, 7, 344-348.