The full evaporation technique: A promising alternative for residual solvents analysis in solid samples

Journal of Separation Science

Volumn 28, Issue 4, 2005, Pages 380-386

  Brault, Audrey ^a   Agasse, Valérie ^a   Cardinael, Pascal ^a,b   Combret, Jean Claude ^a  

^a UNIVERSITÉ DE ROUEN   (France)

^b NONE   (France)

Author keywords

Full evaporation technique; Permethylated cyclodextrin; Residual solvents; Static headspace

Indexed keywords

ACETONE; DRUG PRODUCTS; ENVIRONMENTAL IMPACT; IMPURITIES; METHANOL; SOLVENTS; VOLATILE ORGANIC COMPOUNDS;

ENVIRONMENTAL MATRICES; RESIDUAL SOLVENTS; STATIC HEADSPACE TECHNIQUES; VOLATILE IMPURITIES;

EVAPORATION;

2 BUTANONE; 2 PROPANOL; ACETIC ACID ETHYL ESTER; ACETONE; ACETYLSALICYLIC ACID; ALCOHOL; BETA CYCLODEXTRIN; BUTANOL; ISOBUTANOL; SOLVENT; TETRAHYDROFURAN; VOLATILE AGENT;

ACCURACY; ARTICLE; CALCULATION; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; FULL EVAPORATION TECHNIQUE; GAS CHROMATOGRAPHY; HIGH TEMPERATURE PROCEDURES; LINEAR SYSTEM; MEDICAL LITERATURE; METHYLATION; PRIORITY JOURNAL; SENSITIVITY ANALYSIS; SEPARATION TECHNIQUE; VAPORIZATION;

BETA-CYCLODEXTRINS; CHROMATOGRAPHY; METHYLATION; SOLVENTS; VOLATILIZATION;

EID: 16844372084     PISSN: 16159306     EISSN: None     Source Type: Journal    
DOI: 10.1002/jssc.200401851     Document Type: Article

References (15)

1. International Conference on Harmonisation of Technical Requirements for Registration of Pharmaceuticals for Human Use, ICH Harmonised Tripartite Guideline Q3C Impurities: Guideline for Residual Solvents (Brussels, July 1997).
2. European Pharmacopoeia, 2000. Identification and control of residual solvents. In: European Pharmacopoeia Supplement 2000, European Department for the Quality of Medicines within the Council of Europe, Strasbourg, Section 2.4.24, 32-36.
3. J. Szejtli, Cyclodextrin Technology, Kluwer Academic Publisher, Dordrecht 1988.
4. B. Kolb, L. Ettre, Static Headspace-Gas Chromatography Theory and Practice, Wiley-VCH, Weinheim 1997.
5. N. Kumar, J.G. Gow, J. Chromatogr. 1994, 667 235-240.
6. M.V. Russo, Chromatographia 1994, 39, 645-648.
7. R.B. George, P.D. Wright, Anal. Chem. 1997, 69 2221-2223.
8. P. Cardinaël, V. Peulon-Agasse, G. Coquerel, Y. Combret, J.C. Combret, J. Sep. Sci. 2001, 24, 109-115.
9. M. Markelov, J.P. Guzowski, Anal. Chim. Acta 1993 276, 235-245.
10. J. Schuberth, Anal. Chem. 1996, 68, 1317-1320.
11. J. Schuberth, J. Chromatogr. Sci 1996, 34, 314-319.
12. S. Strassnig, E.P. Lankmayr, J. Chromatogr. A 1999 849, 629-636.
13. J.D. Stuart, M.E. Miller, M.L. Williams-Burnett, J. Soil Contamination 1997, 6, 439-463.
14. V. Schurig, M. Jung, D. Schmalzing, M. Schleimer, J. High Resol. Chromatogr. 1990, 13, 470-474.
15. L. Hong, H.R. Altorfer, Pharmaceutica Acta Helvetiae 1997, 72, 95-104.