X-ray diffraction and solid-state 119Sn CP-MAS NMR studies of some triaryltin(IV) chlorides

Canadian Journal of Chemistry

Volumn 81, Issue 11, 2003, Pages 1187-1195

  Geller, Jordan M ^a   Butler, Ian S ^a   Gilson, Denis F R ^a   Morin, Frederick G ^a   Wharf, Ivor ^a   Belanger Gariepy F ^b  

^a MCGILL UNIVERSITY   (Canada)

^b UNIVERSITÉ DE MONTRÉAL   (Canada)

Author keywords

119Sn chemical shift tensor; Aryltin chlorides; Crystal structure; Magic angle spinning NMR; Tin chlorine spin spin coupling

Indexed keywords

APPROXIMATION THEORY; CHLORINE COMPOUNDS; CRYSTAL SYMMETRY; LIGHT POLARIZATION; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PERTURBATION TECHNIQUES; TENSORS; X RAY DIFFRACTION ANALYSIS;

CROSS POLARIZATION (CS); MAGIC ANGLE SPINNING (MAS); MOLECULAR SYMMETRY; SOLID STATE REACTIONS;

ORGANOMETALLICS;

CHLORIDE; FUNCTIONAL GROUP; RADIOISOTOPE; STRONTIUM 119; UNCLASSIFIED DRUG;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLIZATION; NUCLEAR MAGNETIC RESONANCE; SOLID STATE; STRUCTURE ANALYSIS; TEMPERATURE DEPENDENCE; VALIDATION PROCESS; X RAY CRYSTALLOGRAPHY; X RAY DIFFRACTION;

EID: 1642499262     PISSN: 00084042     EISSN: None     Source Type: Journal    
DOI: 10.1139/v03-115     Document Type: Article

References (38)

1. C.J. Evans and S. Karpel. J. Organomet. Chem. Libr. 16, 135 (1985), and refs. therein.
2. I. Wharf, H. Lamparski, and R. Reeleder. Appl. Organomet. Chem. 11, 969 (1997).
3. I. Wharf. Appl. Organomet. Chem. 14, 34 (2000).
4. I. Wharf. Can. J. Spectrosc. 31, 27 (1986).
5. I. Wharf, A. Bastone, and E.J. Bures. Can. J. Appl. Spectrosc. 41, 122 (1996).
6. D.W. Allen, J.S. Brookes, and R. Formstone. J. Organomet. Chem. 172, 299 (1979).
7. B. King, H. Eckert, D.Z. Denney, and R.H. Herber. Inorg. Chim. Acta, 122, 45 (1986).
8. I. Wharf. Inorg. Chim. Acta, 159, 41 (1989).
9. I. Wharf and M.G. Simard. J. Organomet. Chem. 532, 1 (1997).
10. R.K. Harris and A.C. Olivieri. Prog. Nucl. Magn. Reson. Spectrosc. 24, 435 (1992).
11. A.S. Batsanov, S.M. Cornet, L.A. Crowe, K.B. Dillon, R.K. Harris, P. Hazendonk, and M.D. Roden. Eur. J. Inorg. Chem. 7, 1729 (2001).
12. P. Pyykko. Z. Naturforsch. 47a, 189 (1992).
13. C.J. Jameson. Multinuclear NMR spectroscopy. Edited by J. Mason. Plenum, New York. p. 625. 1987.
14. A.C. Olivieri J. Magn. Reson. 81, 201 (1989).
15. R.A. Komorski, R.G. Parker, and A.M. Mazany. J. Magn. Reson. 73, 389 (1987).
16. R.K. Harris. J. Magn. Reson. 78, 389 (1988).
17. R.K. Harris, A. Sebalt, D. Furlani, and G. Tagliavini. Organometallics, 7, 388 (1988).
18. D.C. Apperley, B. Haiping, and R.K. Harris. Mol. Phys. 68, 1277 (1989).
19. J.S. Tse, F.L. Lee, and E.J. Gabe. Acta Crystallogr. Sect. C, C42, 1876 (1986).
20. T.S. Srivastava. J. Organomet. Chem. 10, 373 (1967).
21. P.J. Green and J.D. Graybeal. J. Am. Chem. Soc. 87, 4305 (1967).
22. S. Alarcón, A.C. Olivieri, and R.K. Harris. Solid State Nucl. Magn. Reson. 2, 325 (1993).
23. B.A. Dunell and S.E. Ulrich. J. Chem. Soc., Faraday Trans. 2, 69, 377 (1973).
24. I. Wharf and A.-M. Lebuis. Acta Crystallogr. Sect. C, C52, 3025 (1996).
25. J. Geller, I. Wharf, F. Bélanger-Gariépy, A.-M. Lebuis, I.S. Butler, and D.F.R. Gilson. Acta Crystallogr., Sect. C, C58, m466 (2002).
26. I. Wharf, A.-M. Lebuis, and G.A. Roper. Inorg. Chim. Acta, 294, 224 (1999).
27. H. Bai, R.K. Harris, and H. Reuter. J. Organomet. Chem. 408, 167 (1991).
28. A. Bondi. J. Phys. Chem. 68, 441 (1964).
29. J. Herzfeld and A.E. Berger. J. Chem. Phys. 73, 6021 (1980).
30. K. Eichele and R.E. Wasylishen. HBA version 1.44 [computer program]. Dalhousie University, Halifax, Nova Scotia. 2001.
31. XPREP, Release 5.10 [computer program]. X-ray data preparation and reciprocal space exploration program. Bruker AXS Inc., Madison, Wis. 53719-1173. 1997.
32. SADABS [computer program]. Bruker area detector absorption corrections. Bruker AXS Inc., Madison, Wis. 1996.
33. G.M. Sheldrick. SHELXS-97 [computer program]. Program for the solution of crystal structures. University of Göttingen, Göttingen, Germany. 1997.
34. G.M. Sheldrick. SHELXL-96 [computer program]. Program for the refinement of crystal structures. University of Göttingen, Göttingen, Germany. 1997.
35. A.J.C. Wilson (Editor). International tables for crystallography. Vol. C4. Kluwer Academic Publishers, Boston. Tables 4.2.6.8 and 6.1.1. 1992.
36. I. Wharf and M.G. Simard. Inorg. Chim. Acta, 282, 30 (1998).
37. F. Huber, A. Saxena, R.K. Harris, and A. Sebald. J. Organomet. Chem. 368, 31 (1989).
38. R. Gobetto, R.K. Harris, and D.C. Apperley. J. Magn. Reson. 96, 119 (1992).