Half-sandwich rhenium(III) acyl complexes: Synthesis, structure and conversion to rhenium(I) and rhenium(III) isonitrile complexes 1

Journal of Organometallic Chemistry

Volumn 524, Issue 1-2, 1996, Pages 133-146

  Filippou, Alexander C ^b   Lungwitz, Bernhard ^a,b   Kociok Köhn, Gabriele ^b   Hinz, Isolde ^b  

^a MASSACHUSETTS INSTITUTE OF TECHNOLOGY   (United States)

^b HUMBOLDT UNIVERSITY   (Germany)

Author keywords

Alkyl complexes; Isonitrile complexes; Rhenium

Indexed keywords

EID: 16144367859     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(96)06401-7     Document Type: Article

References (66)

1. [1] J.P. Collman, L.S. Hegedus, J.R. Norton and R.G. Finke, Principles and Applications of Organotransition Metal Chemistry, University Science Books, Mill Valley, USA, 1987.
2. [2] (a) W. Hieber, G. Braun and W. Beck, Chem. Ber., 93 (1960) 901;
3. (b) H.D. Kaesz, R.B. King and F.G.A. Stone, Z. Naturforsch., 15b (1960) 763;
4. (c) A.N. Nesmeyanov, K.N. Anisimov, N.B. Kolobova and A.A. Ioganson, Dokl. Chem., 175 (1967) 742;
5. (d) D.J. Desrosiers and R.P. Hugles, J. Am. Chem. Soc., 103 (1981) 5593;
6. (e) M.J. Schweiger, U. Nagel and W. Beck, J. Organomet. Chem., 355 (1988) 289;
7. (f) J.M. Andersen and J.R. Moss, J. Organomet. Chem., 494 (1995) 105.
8. [3] (a) T. Kruck and M. Noack, Chem. Ber., 97 (1964) 1693;
9. (b) A.M. Brodie, G. Hulley, B.F.G. Johnson and J. Lewis, J. Organomet. Chem., 24 (1970) 201.
10. [4] (a) R.W. Brink and R.J. Angelici, Inorg. Chem., 12 (1973) 1062;
11. (b) R.J. Angelici and R.W. Brink, Inorg. Chem., 12 (1973) 1067;
12. (c) H. Behrens, R.-J. Lampe, P. Merbach and M. Moll, J. Organomet. Chem., 159 (1978) 201.
13. [5] (a) H. Behrens, E. Lindner and P. Pässler, Z. Anorg. Allg. Chem., 365 (1969) 137;
14. (b) R.J. Angelici and A.E. Kruse, J. Organomet. Chem., 22 (1970) 461;
15. (c) C.M. Lukehart and J.V. Zeile, J. Am. Chem. Soc., 98 (1976) 2365;
16. (d) K.P. Darst and C.M. Lukehart, J. Organomet. Chem., 171 (1979) 65;
17. (e) A.C. Filippou, E.O. Fischer, G. Müller and H.G. Alt, J. Organomet. Chem., 329 (1987) 223;
18. (f) S. Feracin, H.-U. Hund, H.W. Bosch, E. Lippmann, W. Beck and H. Berke, Helv. Chim. Acta, 75 (1992) 1305.
19. [6] E.O. Fischer and A. Riedel, Chem. Ber., 101 (1968) 156.
20. [7] (a) E.O. Fischer, E. Offhaus, J. Müller and D. Nöthe, Chem. Ber., 105 (1972) 3027;
21. (b) E.O. Fischer, T.L. Lindner, H. Fischer, G. Huttner, P. Friedrich and F.R. Kreißl, Z. Naturforsch., 32b (1977) 648.
22. [8] (a) C.P. Casey, C.R. Cyr, R.L. Anderson and D.F. Marten, J. Am. Chem. Soc., 97 (1975) 3053;
23. (b) C.P. Casey and D.M. Scheck, J. Am. Chem. Soc., 102 (1980) 2723.
24. [9] (a) A.N. Nesmeyanov, N.E. Kolobova, Y.V. Makarov, E.I. Kazimirchuk and K.N. Anisimov, Izv. Akad. Nauk SSSR, Ser. Khim., (1976) 159;
25. (b) K.I. Goldberg and R.G. Bergman, J. Am. Chem. Soc., 111 (1989) 1285.
26. [10] E.O. Fischer, C. Apostolidis, E. Dornberger, A.C. Filippou, B. Kanellakopulos, B. Lungwitz, J. Müller, B. Powietzka, J. Rebizant and W. Roth, Z. Naturforsch., 50b (1995) 1382.
27. [11] (a) E.O. Fischer, W. Held, F.R. Kreißl, A. Frank and G. Huttner, Chem. Ber., 110 (1977) 656;
28. (b) C.P. Casey and T.J. Burkhardt, C.A. Bunnell and J.C. Calabrese, J. Am. Chem. Soc., 99 (1977) 2127.
29. [12] (a) E.O. Fischer, R.L. Clough and P. Stückler, J. Organomet. Chem., 120 (1976) C6;
30. (b) E.O. Fischer and A. Frank, Chem. Ber., 111 (1978) 3740.
31. [13] (a) E.O. Fischer, R.L. Clough, G. Besl and F.R. Kreißl, Angew. Chem, 88 (1976) 584;
32. Angew. Chem., Int. Ed. Engl., 15 (1976) 543.
33. [14] W.A. Herrmann, Chem. Ber., 108 (1975) 486.
34. [15] (a) C.P. Casey, R.A. Boggs and R.L. Anderson, J. Am. Chem. Soc., 94 (1972) 8947;
35. (b) E.O. Fischer and S. Riedmüller, Chem. Ber., 107 (1974) 915;
36. (c) C.M. Lukehart and J.V. Zeile, J. Organomet. Chem., 97 (1975) 421;
37. (d) W.D. Wulff and D.C. Yang, J. Am. Chem. Soc., 105 (1983) 6726.
38. [16] C.J. Pouchert (ed.), The Aldrich Library of FT-IR Spectra, Vol. 2, 1985, p. 340.
39. [17] (a) C.-F. Barrientos-Penna, F.W.B. Einstein, D. Sutton and A.C. Willis, Inorg. Chem., 19 (1980) 2740;
40. (b) F.W.B. Einstein, A.H. Klahn-Oliva, D. Sutton and K.G. Tyers, Organometallics, 5 (1986) 53.
41. [18] (a) N.E. Kolobova, Z.P. Zalueva and E.I. Kazimirchuk, Izv. Akad. Nauk SSSR, Ser. Khim., (1981) 408;
42. (b) R.B. King, J. Inorg. Nucl. Chem., 29 (1967) 2119.
43. [19] (a) A.N. Nesmeyanov, N.E. Kolobova, Y.V. Makarov and K.N. Anisimov, Izv. Akad. Nauk SSSR, Ser. Khim., (1969) 1826;
44. (b) R.B. King, R.H. Reimann and D.J. Darensbourg, J. Organomet. Chem., 93 (1975) C23;
45. (c) R.B. King and R.H. Reimann, Inorg. Chem., 15 (1976) 183.
46. [20] M.R. Terry, L.A. Mercando, C. Kelley, G.L. Geoffroy, P. Nombel, N. Lugan, R. Mathieu, R.L. Ostrander, B.E. Owens-Waltermire and A.L. Rheingold, Organometallics, 13 (1994) 843.
47. [21] (a) A.H. Klahn-Oliva, R.D. Singer, J.M. Aramini and D. Sutton, Inorg. Chem., 28 (1989) 4217;
48. (b) C. Leiva, K. Mossert, A.H. Klahn and D. Sutton, J. Organomet. Chem., 469 (1994) 69.
49. [22] L.J. Todd and J.R. Wilkinson, J. Organomet. Chem., 77 (1974) 1.
50. [23] M.J. Webb and W.A.G. Graham, J. Organomet. Chem., 93 (1975) 119.
51. [24] P. Kubacek, R. Hoffmann and Z. Havlas, Organometallics, 1 (1982) 180.
52. [25] M.R. Churchill, K.N. Amoh and H.J. Wasserman, Inorg. Chem., 20 (1981) 1609.
53. [26] A.S. Foust, J.K. Hoyano and W.A.G. Graham, J. Organomet. Chem., 32 (1971) C65.
54. [27] F. Calderazzo, I.P. Mavani, D. Vitali, I. Bernal, J.D. Korp and J.L. Atwood, J. Organomet. Chem., 160 (1978) 207.
55. [28] J.L. Atwood, J.K. Newell, W.E. Hunter, I. Bernal, F. Calderazzo, I.P. Mavani and D. Vitali, J. Chem. Soc., Chem. Commun., (1976) 441.
56. [29] J.D. Korp, I. Bernal, J.L. Atwood, F. Calderazzo and D. Vitali, J. Chem. Soc., Dalton Trans., (1979) 1492.
57. [30] R.L. Davis and N.C. Baenziger, Inorg. Nucl. Chem. Lett., 13 (1977) 475.
58. [31] H.J. Lucas and E.R. Kennedy, Org. Synth. Collect., 3 (1976) 482.
59. [32] (a) J. Casanova, Jr., R.E. Schuster and N.D. Werner, J. Chem. Soc., (1963) 4280;
60. (b) R.E. Schuster, J.E. Scott and J. Casanova, Jr., Org. Synth., 46 (1966) 75.
61. [33] M. Veith and H. Bärnighausen, Acta Crystallogr. B, 30 (1974) 1806.
62. [34] G.M. Sheldrick, SHELXS-86, Program for Crystal Structure Solution, Universität Göttingen, Germany, 1986.
63. [35] G.M. Sheldrick, SHELX-93, Program for Crystal Structure Determination, University of Cambridge, UK, 1993.
64. [36] D.T. Cromer and J.B. Mann, Acta Crystallogr. A, 24 (1968) 321.
65. [37] (a) A.L. Spek, PLUTON-92 and PLATON-93, Graphics program, Universität Utrecht, Netherlands, 1992 and 1993;
66. (b) A.L. Spek, Acta Crystallogr. A, 46 (1990) C34.