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64 originating from possible radical-radical interactions. In most cases we did not detect any additional EPR signal in that region. Only in cases where the samples were incubated at alkaline pH for long periods, i.e., 4 h or more, the g 2 EPR signals showed splittings accompanied by formation of g 4 "forbidden" transitions (data not shown). Thus, at prolonged incubation times, dimeric and then polymeric species start to form from the monomeric radicals. On the contrary, the radicals presented in Figure 3, formed under short incubation period, are monomeric radicals.
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