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15944367824
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note
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A nonsolvated crystal of 17 {triclinic, P1̄, a = 10.848(2) Å, b = 14.295(3) Å, c = 24.476(5) Å, α = 75.34(2)°, β= 88.90(2)°, γ = 89.17-(2)°} was also analyzed by XRD establishing the presence of molecules very similar to that of Figure 8: the lattice contained two independent molecules per unit cell, one with disorder at the hydroxyl group, but refinement of the data gave high final A factors {indices [I>2σ(I)]: R1 = 0.1129, wR2 = 0.2677; all indices R1 = 0.1260, wR2 = 0.2702}. See Supporting Information.
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