The first fully sandwiched lithiacarborane complex: A synthetic and structural investigation

Journal of the American Chemical Society

Volumn 118, Issue 21, 1996, Pages 5150-5151

  Hosmane, Narayan S ^a   Yang, Jimin ^a   Zhang, Hongming ^a   Maguire, John A ^a  

^a SOUTHERN METHODIST UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

MOLECULAR STRUCTURE; ORGANOMETALLICS; SYNTHESIS (CHEMICAL);

LITHIACARBORANE COMPLEXES; SANDWICHED COMPLEXES;

LITHIUM COMPOUNDS;

CARBORANE DERIVATIVE; LIGAND; LITHIACARBORANE; LITHIUM; SODIUM; UNCLASSIFIED DRUG;

ARTICLE; DRUG STABILITY; DRUG STRUCTURE; DRUG SYNTHESIS; INFRARED SPECTROMETRY; OXIDATION; PROTON NUCLEAR MAGNETIC RESONANCE; X RAY ANALYSIS; X RAY CRYSTALLOGRAPHY;

EID: 15844384181     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja9602915     Document Type: Article

References (19)

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12. 2.
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15. 2 (2): C, 49.19; H, 11.50; N, 8.09. Found: C, 49.32; H, 11.33; N, 8.04. The yellow polymeric mass that remained in the reaction flask after complete sublimation of 2 was insoluble in organic solvents and, therefore, was discarded.
16. 2 (2): C, 49.19; H, 11.50; N, 8.09. Found: C, 49.32; H, 11.33; N, 8.04. The yellow polymeric mass that remained in the reaction flask after complete sublimation of 2 was insoluble in organic solvents and, therefore, was discarded.
17. Cotton, F. A.; Wilkinson, G. Advanced Inorganic Chemistry, 5th ed.; Wiley: New York, 1988.
18. 6) 2552.1 (w, br), 2394.1 (m, s), 2288.8 (vvs) [v-(B-H)], 1867.6 (m, br) [B-H-B (bridge)].
19. w = 0.079, and GOF = 1.58.